1,3-Benzodioxol-5-aMine, 6-iodo-

Product Name: 1,3-Benzodioxol-5-aMine, 6-iodo-
CAS No.: 1000802-34-5
Chemical Name: 1,3-Benzodioxol-5-aMine, 6-iodo-
Synonyms: 5-Amino-6-iodo-1,3-benzodioxole; 6-Iodo-1,3-benzodioxol-5-amine;1,3-Benzodioxol-5-aMine, 6-iodo-;6-iodobenzo[d][1,3]dioxol-5-aMine;6-Iodo-benzo[1,3]dioxol-5-ylamine
CBNumber: CB92614518
Molecular Formula: C7H6INO2
Formula Weight: 263.03
MOL File: 1000802-34-5.mol

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1,3-Benzodioxol-5-aMine, 6-iodo- Property

storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
Appearance: Light yellow to brown Solid

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Safety

HS Code: 2932990090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Apolloscientific

Product number: OR370010
Product name: 6-Iodobenzo[d][1,3]dioxol-5-amine
Packaging: 250mg
Price: $387
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0368137
Product name: 6-IODOBENZO[D][1,3]DIOXOL-5-AMINE
Purity: 95.00%
Packaging: 5MG
Price: $502.03
Updated: 2021/12/16

Ark Pharm

Product number: AK127270
Product name: 6-Iodobenzo[d][1,3]dioxol-5-amine
Purity: 95+%
Packaging: 100mg
Price: $64
Updated: 2021/12/16

Ambeed

Product number: A232480
Product name: 6-Iodobenzo[d][1,3]dioxol-5-amine
Purity: 95+%
Packaging: 250mg
Price: $113
Updated: 2021/12/16

Ambeed

Product number: A232480
Product name: 6-Iodobenzo[d][1,3]dioxol-5-amine
Purity: 95+%
Packaging: 100mg
Price: $57
Updated: 2021/12/16

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1,3-Benzodioxol-5-aMine, 6-iodo- Chemical Properties,Usage,Production

Synthesis

1000802-33-4

1000802-34-5

N-(6-Iodobenzo[d][1,3]dioxol-5-yl)acetamide (200 mg, 0.656 mmol) was used as a raw material, which was dissolved with NaOH (1.31 g, 32.8 mmol) in a solvent mixture of ethanol (26 mL) and water (6 mL). The reaction mixture was heated to reflux under stirring and kept for 4 hours. Upon completion of the reaction, the mixture was cooled and the solvent was evaporated under reduced pressure. The residue was extracted by partitioning with dichloromethane (100 mL) and water (100 mL). The organic layer was separated and washed with distilled water (2 x 100 mL). The organic layer was dried over anhydrous magnesium sulfate and concentrated under reduced pressure to afford 6-iodobenzo[d][1,3]dioxol-5-amine (170 mg, 98% yield) as an orange solid. The product was analyzed by LC-MS showing [M+1]+ m/z 264; 1H NMR (DMSO-d6) δ 4.88 (s, 2H), 5.87 (s, 2H), 6.47 (s, 1H), 7.07 (s, 1H).

References

[1] Patent: US2008/234314, 2008, A1. Location in patent: Page/Page column 59
[2] Patent: US2010/184801, 2010, A1
[3] Patent: US2016/317508, 2016, A1. Location in patent: Paragraph 0181
[4] Patent: WO2008/47109, 2008, A1. Location in patent: Page/Page column 56
[5] Journal of Medicinal Chemistry, 2015, vol. 58, # 9, p. 3922 - 3943

1,3-Benzodioxol-5-aMine, 6-iodo- Preparation Products And Raw materials

Raw materials

Preparation Products

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1,3-Benzodioxol-5-aMine, 6-iodo- Suppliers

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View Lastest Price from 1,3-Benzodioxol-5-aMine, 6-iodo- manufacturers

Career Henan Chemical Co

Product: 6-Iodo-1,3-benzodioxol-5-amine 1000802-34-5
Price: US $1.00/KG
Min. Order: 1KG
Purity: Min98% HPLC
Supply Ability: g/kg/ton
Release date: 2020-02-05

1000802-34-5, 1,3-Benzodioxol-5-aMine, 6-iodo-Related Search:

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1000802-34-5