6-BroMo-2-Methyl-nicotinic acid
- Product Name
- 6-BroMo-2-Methyl-nicotinic acid
- CAS No.
- 1060805-97-1
- Chemical Name
- 6-BroMo-2-Methyl-nicotinic acid
- Synonyms
- 6-BroMo-2-Methyl-nicotinic acid;6-Bromo-2-methylpyridine-3-carboxylic acid;6-bromo-2-methyl-3-Pyridinecarboxylic acid;3-Pyridinecarboxylic acid, 6-bromo-2-methyl-
- CBNumber
- CB92642371
- Molecular Formula
- C7H6BrNO2
- Formula Weight
- 216.03
- MOL File
- 1060805-97-1.mol
6-BroMo-2-Methyl-nicotinic acid Property
- Boiling point:
- 332.7±42.0 °C(Predicted)
- Density
- 1.692±0.06 g/cm3(Predicted)
- storage temp.
- Inert atmosphere,Room Temperature
- pka
- 2.90±0.25(Predicted)
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- B808405
- Product name
- 6-Bromo-2-methylnicotinicAcid
- Packaging
- 500mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- Y3603
- Product name
- 6-Bromo-2-methylpyridine-3-carboxylicacid
- Packaging
- 5g
- Price
- $4787
- Updated
- 2021/12/16
- Product number
- NP1105
- Product name
- 6-Bromo-2-methyl-nicotinicacid
- Purity
- >95%
- Packaging
- 1g
- Price
- $280
- Updated
- 2021/12/16
- Product number
- BB20-7345
- Product name
- 6-Bromo-2-methyl-nicotinicacid
- Purity
- 95%
- Packaging
- 1g
- Price
- $285
- Updated
- 2021/12/16
- Product number
- CD11358170
- Product name
- 6-Bromo-2-methylnicotinicacid
- Purity
- 98%
- Packaging
- 1g
- Price
- $465
- Updated
- 2021/12/16
6-BroMo-2-Methyl-nicotinic acid Chemical Properties,Usage,Production
Synthesis
926293-55-2
1060805-97-1
Step 13b. 6-Bromo-2-methylnicotinic aldehyde (Compound 1102, 1.4 g, 6.7 mmol) was taken as raw material and dissolved in acetone (20 mL) at 0 °C and Jones reagent (2.67 M, 5.2 ml) was added slowly with stirring. The reaction mixture was gradually warmed up to room temperature and stirring was continued for 30 min. After completion of the reaction, the pH of the reaction solution was adjusted to 5-6 with saturated NaHCO3 solution. the reaction mixture was extracted with ethyl acetate, the organic layers were combined, washed with brine, dried over anhydrous sodium sulfate and concentrated. The crude product was purified by silica gel column chromatography with the eluent ethyl acetate/hexane (1:8) to afford 6-bromo-2-methylnicotinic acid (Compound 1103, 1.0 g, 66% yield) as a white solid.1H NMR (400 MHz, CDCl3): δ 2.87 (s, 3H), 7.46 (d, J=8.4 Hz, 1H), 8.15 (d, J= 8.4Hz, 1H).
References
[1] Patent: US2014/18368, 2014, A1. Location in patent: Paragraph 0162; 0242
6-BroMo-2-Methyl-nicotinic acid Preparation Products And Raw materials
Raw materials
Preparation Products
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