2,6-Dichloro-4-cyanobenzoic acid
- Product Name
- 2,6-Dichloro-4-cyanobenzoic acid
- CAS No.
- 1258298-05-3
- Chemical Name
- 2,6-Dichloro-4-cyanobenzoic acid
- Synonyms
- 4-Cyano-2,6-dichlorobenzoic acid;4-Carboxy-3,5-dichlorobenzonitrile;Benzoic acid, 2,6-dichloro-4-cyano-;4-Cyano-2,6-dichlorobenzoic acid 95%;2,6-dichloro-4-cyanobenzoic acid methyl ester
- CBNumber
- CB92648186
- Molecular Formula
- C8H3Cl2NO2
- Formula Weight
- 216.02
- MOL File
- 1258298-05-3.mol
2,6-Dichloro-4-cyanobenzoic acid Property
- Boiling point:
- 337.6±42.0 °C(Predicted)
- Density
- 1.62
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 0.86±0.25(Predicted)
- Appearance
- White to off-white Solid
- InChI
- InChI=1S/C8H3Cl2NO2/c9-5-1-4(3-11)2-6(10)7(5)8(12)13/h1-2H,(H,12,13)
- InChIKey
- RABGVNSIHQKYAS-UHFFFAOYSA-N
- SMILES
- C(O)(=O)C1=C(Cl)C=C(C#N)C=C1Cl
Safety
- HS Code
- 2926907090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
N-Bromosuccinimide Price
- Product number
- D439303
- Product name
- 2,6-Dichloro-4-cyanobenzoicacid
- Packaging
- 50mg
- Price
- $200
- Updated
- 2021/12/16
- Product number
- HCH0062785
- Product name
- 2,6-DICHLORO-4-CYANOBENZOIC ACID
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $504.17
- Updated
- 2021/12/16
- Product number
- 101574
- Product name
- 2,6-Dichloro-4-cyanobenzoic acid
- Purity
- 97%
- Packaging
- 1g
- Price
- $615
- Updated
- 2021/12/16
- Product number
- 4637-5-04
- Product name
- 4-Cyano-2,6-dichlorobenzoic acid
- Purity
- 95%
- Packaging
- 500mg
- Price
- $640
- Updated
- 2021/12/16
- Product number
- 4637-5-04
- Product name
- 4-Cyano-2,6-dichlorobenzoic acid
- Purity
- 95%
- Packaging
- 1g
- Price
- $960
- Updated
- 2021/12/16
2,6-Dichloro-4-cyanobenzoic acid Chemical Properties,Usage,Production
Synthesis
409127-32-8
1258298-05-3
Step b: Synthesis of 2,6-dichloro-4-cyanobenzoic acid Methyl 2,6-dichloro-4-cyanobenzoate (620 mg, 2.6 mmol) was suspended in pyridine (5 mL) and anhydrous lithium iodide (1000 mg, 8 mmol) was added. The reaction mixture was heated and stirred at reflux for 1 h, followed by concentration under reduced pressure to remove the pyridine. The residue was acidified to pH 2-3 with 2N hydrochloric acid under cooling in an ice bath.The precipitated solid was filtered, washed with water and dried to afford 2,6-dichloro-4-cyanobenzoic acid (380 mg, 86% yield) as a light brown solid.1H NMR (400 MHz, DMSO-d6): δ 8.23 (s, 2H).
References
[1] Patent: WO2012/160464, 2012, A1. Location in patent: Page/Page column 78
[2] Patent: US2014/155398, 2014, A1. Location in patent: Paragraph 0469; 0470
[3] Patent: US2010/317643, 2010, A1. Location in patent: Page/Page column 101
[4] Journal of Medicinal Chemistry, 2013, vol. 56, # 11, p. 4521 - 4536
2,6-Dichloro-4-cyanobenzoic acid Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2,6-Dichloro-4-cyanobenzoic acid manufacturers
- Product
- 2,6-Dichloro-4-cyanobenzoic acid 1258298-05-3
- Price
- US $3500.00-3100.00/KG
- Min. Order
- 1G
- Purity
- 99%
- Supply Ability
- 100kg
- Release date
- 2018-08-03