ChemicalBook > CAS DataBase List > 6-BroMo-n,n-diMethylpyridine-3-aMine

6-BroMo-n,n-diMethylpyridine-3-aMine

Product Name: 6-BroMo-n,n-diMethylpyridine-3-aMine
CAS No.: 39856-56-9
Chemical Name: 6-BroMo-n,n-diMethylpyridine-3-aMine
Synonyms: 6-broMo-N,N-diMethylpyridin-3-aMine;6-BroMo-n,n-diMethylpyridine-3-aMine;(6-BroMo-pyridin-3-yl)-diMethyl-aMine;3-PyridinaMine, 6-broMo-N,N-diMethyl-;6-bromo-N,N-dimethylpyridin-3-amine,2-bromo-5-dimethylaminopyridine
CBNumber: CB92651726
Molecular Formula: C7H9BrN2
Formula Weight: 201.06
MOL File: 39856-56-9.mol

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6-BroMo-n,n-diMethylpyridine-3-aMine Property

Melting point:: 64-66 °C(Solv: hexane (110-54-3))
Boiling point:: 278.8±20.0 °C(Predicted)
Density: 1.469±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 1.96±0.22(Predicted)
Appearance: Off-white to yellow Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: B593625
Product name: 6-bromo-N,N-dimethylpyridin-3-amine
Packaging: 50mg
Price: $90
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB142462
Product name: 6-Bromo-N,N-dimethylpyridin-3-amine
Packaging: 1g
Price: $98
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB142462
Product name: 6-Bromo-N,N-dimethylpyridin-3-amine
Packaging: 2g
Price: $171
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0118315
Product name: 2-BROMO-5-N-(DIMETHYLAMINE)-PYRIDINE
Purity: 95.00%
Packaging: 5MG
Price: $495.25
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB142462
Product name: 6-Bromo-N,N-dimethylpyridin-3-amine
Packaging: 10g
Price: $594
Updated: 2021/12/16

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6-BroMo-n,n-diMethylpyridine-3-aMine Chemical Properties,Usage,Production

Synthesis

13534-97-9

74-88-4

39856-56-9

5-Amino-2-bromopyridine (300 mg, 1.73 mmol) was dissolved in tetrahydrofuran (30 mL) under nitrogen protection and cooled to -78 °C. A tetrahydrofuran solution of 1 M bis(trimethylmethylsilyl)lithium amide (3.46 mL, 3.46 mmol) was slowly added to this solution over 6 min. After maintaining -78 °C and stirring for 30 min, iodomethane (566 mg, 3.99 mmol) was added. The reaction mixture was gradually warmed to room temperature and stirring was continued for 1 hour. Upon completion of the reaction, the reaction was quenched with saturated aqueous ammonium chloride solution (50 mL). The reaction mixture was extracted with ethyl acetate (3 x 50 mL) and the organic phases were combined. The organic phase was washed sequentially with brine (2 x 50 mL) and dried over anhydrous sodium sulfate. After filtration, the filtrate was concentrated under reduced pressure and the resulting residue was purified by silica gel column chromatography with the eluent being a petroleum ether solution of 1-10% ethyl acetate to give 6-bromo-N,N-dimethylpyridin-3-amine as a light yellow solid. Mass spectrum (ESI, m/z): 201.0,203.0 [M + 1]+.

References

[1] Patent: WO2015/188368, 2015, A1. Location in patent: Page/Page column 54

6-BroMo-n,n-diMethylpyridine-3-aMine Preparation Products And Raw materials

Raw materials

Preparation Products

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39856-56-9, 6-BroMo-n,n-diMethylpyridine-3-aMineRelated Search:

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39856-56-9