6-broMo-1-Methyl-1H-pyrrolo[3,2-b]pyridine6-broMo-1-Methyl-1H-pyrrolo[3,2-b]pyridine
- Product Name
- 6-broMo-1-Methyl-1H-pyrrolo[3,2-b]pyridine6-broMo-1-Methyl-1H-pyrrolo[3,2-b]pyridine
- CAS No.
- 1086064-46-1
- Chemical Name
- 6-broMo-1-Methyl-1H-pyrrolo[3,2-b]pyridine6-broMo-1-Methyl-1H-pyrrolo[3,2-b]pyridine
- Synonyms
- 6-Bromo-1-methyl-4-azaindole;1H-Pyrrolo[3,2-b]pyridine, 6-bromo-1-methyl-;6-broMo-1-Methyl-1H-pyrrolo[3,2-b]pyridine6-broMo-1-Methyl-1H-pyrrolo[3,2-b]pyridine
- CBNumber
- CB92655214
- Molecular Formula
- C8H7BrN2
- Formula Weight
- 211.06
- MOL File
- 1086064-46-1.mol
6-broMo-1-Methyl-1H-pyrrolo[3,2-b]pyridine6-broMo-1-Methyl-1H-pyrrolo[3,2-b]pyridine Property
- storage temp.
- 2-8°C
- Appearance
- White to yellow Solid
Safety
- HS Code
- 2933399990
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P310Immediately call a POISON CENTER or doctor/physician.
N-Bromosuccinimide Price
- Product number
- 3H32-9-8B
- Product name
- 6-Bromo-1-methyl-1H-pyrrolo[3,2-b]pyridine
- Purity
- 95.0%
- Packaging
- 250mg
- Price
- $117
- Updated
- 2021/12/16
- Product number
- OR301261
- Product name
- 6-Bromo-1-methyl-1H-pyrrolo[3,2-b]pyridine
- Packaging
- 250mg
- Price
- $99
- Updated
- 2021/12/16
- Product number
- CM149588
- Product name
- 6-bromo-1-methyl-1H-pyrrolo[3,2-b]pyridine
- Purity
- 95%+
- Packaging
- 100mg
- Price
- $113
- Updated
- 2021/12/16
- Product number
- A312440
- Product name
- 6-Bromo-1-methyl-1H-pyrrolo[3,2-b]pyridine
- Purity
- 95%
- Packaging
- 100mg
- Price
- $66
- Updated
- 2021/12/16
- Product number
- A312440
- Product name
- 6-Bromo-1-methyl-1H-pyrrolo[3,2-b]pyridine
- Purity
- 95%
- Packaging
- 250mg
- Price
- $88
- Updated
- 2021/12/16
6-broMo-1-Methyl-1H-pyrrolo[3,2-b]pyridine6-broMo-1-Methyl-1H-pyrrolo[3,2-b]pyridine Chemical Properties,Usage,Production
Synthesis
944937-53-5
74-88-4
1086064-46-1
Step 2: 6-Bromo-4-azaindole (1.0 g, 5 mmol) was dissolved in N,N-dimethylformamide (10 mL) and cooled in an ice bath. Sodium hydride (400 mg, 10 mmol, 60% dispersed in mineral oil) was added slowly with stirring. The ice bath temperature was maintained and stirring was continued for 1 hour. Subsequently, iodomethane (852 mg, 6 mmol) was added dropwise and the reaction mixture was warmed to 25 °C and stirred for 2 hours. Upon completion of the reaction, the reaction was quenched with methanol. The mixture was concentrated to dryness under reduced pressure. The residue was purified by column chromatography (silica gel, 100-200 mesh, eluent: hexane solution of 20% ethyl acetate) to afford 6-bromo-1-methyl-1H-pyrrolo[3,2-b]pyridine (1 g, 95% yield).1H NMR (400 MHz, chloroform-d) δ 8.47 (d, J=2 Hz, 1H), 7.75-7.74 (m, 1H) , 7.25-7.23 (m, 1H), 6.65-6.63 (m, 1H), 3.76 (s, 3H).
References
[1] Patent: WO2016/142310, 2016, A1. Location in patent: Page/Page column 78
[2] Patent: WO2014/11568, 2014, A1. Location in patent: Paragraph 0180; 0181; 0182
[3] Patent: WO2011/110575, 2011, A1. Location in patent: Page/Page column 66
6-broMo-1-Methyl-1H-pyrrolo[3,2-b]pyridine6-broMo-1-Methyl-1H-pyrrolo[3,2-b]pyridine Preparation Products And Raw materials
Raw materials
Preparation Products
6-broMo-1-Methyl-1H-pyrrolo[3,2-b]pyridine6-broMo-1-Methyl-1H-pyrrolo[3,2-b]pyridine Suppliers
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- tp@aladdinsci.com
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- United States
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