2-(tert-butoxy)pyridine

Product Name: 2-(tert-butoxy)pyridine
CAS No.: 83766-88-5
Chemical Name: 2-(tert-butoxy)pyridine
Synonyms: 2-(tert-butoxy)pyridine;Chlorphenamine Impurity 61;2-(1,1-Dimethylethoxy)pyridine;Pyridine, 2-(1,1-dimethylethoxy)-
CBNumber: CB92658750
Molecular Formula: C9H13NO
Formula Weight: 151.21
MOL File: 83766-88-5.mol

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2-(tert-butoxy)pyridine Property

Boiling point:: 88°C/100mmHg(lit.)
Density: 0.967±0.06 g/cm3(Predicted)
refractive index: 1.4840 to 1.4880
storage temp.: Inert atmosphere,Room Temperature
form: clear liquid
pka: 4.25±0.12(Predicted)
color: Colorless to Light yellow to Light orange

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

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N-Bromosuccinimide Price

TCI Chemical

Product number: B5575
Product name: 2-tert-Butoxypyridine
Purity: >98.0%(GC)
Packaging: 1g
Price: $60
Updated: 2026/04/30

TCI Chemical

Product number: B5575
Product name: 2-tert-Butoxypyridine
Purity: >98.0%(GC)
Packaging: 5g
Price: $211
Updated: 2026/04/30

SynQuest Laboratories

Product number: 4H07-1-83
Product name: 2-(tert-Butoxy)pyridine
Packaging: 1g
Price: $292
Updated: 2021/12/16

Matrix Scientific

Product number: 118093
Product name: 2-(tert-Butoxy)pyridine
Packaging: 1g
Price: $200
Updated: 2021/12/16

Chemenu

Product number: CM120976
Product name: 2-(tert-Butoxy)pyridine
Purity: 95%
Packaging: 1g
Price: $128
Updated: 2021/12/16

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2-(tert-butoxy)pyridine Chemical Properties,Usage,Production

Synthesis

109-09-1

865-47-4

83766-88-5

GENERAL STEPS: A mixture of potassium tert-butoxide (9.88 g, 88.07 mmol) and 2-chloropyridine (5 g, 44.04 mmol) was dissolved in toluene (100 mL), followed by the addition of 18-crown-6 (0.58 g, 2.20 mmol) as a phase transfer catalyst. The reaction mixture was stirred and refluxed at 110 °C for 15 hours. After completion of the reaction, the mixture was cooled to room temperature, diluted with ethyl acetate (200 mL) and washed sequentially with water (150 mL) and saturated brine (150 mL). The organic layer was separated, dried with anhydrous sodium sulfate and concentrated under reduced pressure to remove the solvent. The resulting crude product was purified by silica gel column chromatography using gradient elution (0:5 to 1:5 ethyl acetate/hexane) to afford the target compound 2-(tert-butoxy)pyridine (3.59 g, 54%) as a colorless oil. The structure of the product was confirmed by 1H NMR, 13C NMR and high resolution mass spectrometry (HRMS): 1H NMR (400 MHz, CDCl3) δ 8.15 (ddd, J = 4.8, 2.0, 0.4 Hz, 1H), 7.52 (ddd, J = 9.2, 6.8, 1.6 Hz, 1H), 6.81 (ddd, J = 6.8, 5.2, 1.2 Hz, 1H), 6.67 (dt, J = 8.4, 0.8 Hz, 1H), 1.61 (s, 9H); 13C NMR (100 MHz, CDCl3) δ 163.9, 146.5, 138.1, 116.2, 113.4, 79.4, 28.7 (3C); HRMS (ESI) m/z calcd for C9H14NO [M + H]+ 152.1075, found 152.1077.

References

[1] Tetrahedron, 2018, vol. 74, # 27, p. 3748 - 3754
[2] Tetrahedron Letters, 2014, vol. 55, # 51, p. 7133 - 7135

2-(tert-butoxy)pyridine Preparation Products And Raw materials

Raw materials

Preparation Products

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2-(tert-butoxy)pyridine Suppliers

Americas 1 China 54 Europe 1 India 2 Japan 1 United Kingdom 1 United States 6 Global 66

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83766-88-5, 2-(tert-butoxy)pyridineRelated Search:

2-(tert-butoxy)pyridine

Pyridine, 2-(1,1-dimethylethoxy)-

2-(1,1-Dimethylethoxy)pyridine

Chlorphenamine Impurity 61

83766-88-5