(4-Chloro-3-Methoxyphenyl)Methanol

Product Name: (4-Chloro-3-Methoxyphenyl)Methanol
CAS No.: 13726-17-5
Chemical Name: (4-Chloro-3-Methoxyphenyl)Methanol
Synonyms: 4-Chloro-3-methoxybenzyl alcohol;(4-Chloro-3-Methoxyphenyl)Methanol;Benzenemethanol, 4-chloro-3-methoxy-
CBNumber: CB92660959
Molecular Formula: C8H9ClO2
Formula Weight: 172.61
MOL File: 13726-17-5.mol

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(4-Chloro-3-Methoxyphenyl)Methanol Property

Boiling point:: 279.2±25.0 °C(Predicted)
Density: 1.239±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 14.04±0.10(Predicted)
Appearance: White to off-white Solid

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Safety

HS Code: 2909498090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: C372118
Product name: (4-chloro-3-methoxyphenyl)methanol
Packaging: 2.5g
Price: $45
Updated: 2021/12/16

TRC

Product number: C372118
Product name: (4-chloro-3-methoxyphenyl)methanol
Packaging: 25g
Price: $75
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC139974
Product name: (4-Chloro-3-methoxyphenyl)methanol
Packaging: 500mg
Price: $70
Updated: 2021/12/16

AK Scientific

Product number: J96742
Product name: (4-Chloro-3-methoxyphenyl)methanol
Packaging: 1g
Price: $91
Updated: 2021/12/16

AK Scientific

Product number: Y6044
Product name: (4-Chloro-3-methoxyphenyl)methanol
Packaging: 1g
Price: $117
Updated: 2021/12/16

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(4-Chloro-3-Methoxyphenyl)Methanol Chemical Properties,Usage,Production

Synthesis Reference(s)

Journal of Medicinal Chemistry, 32, p. 1757, 1989 DOI: 10.1021/jm00128a016

Synthesis

85740-98-3

13726-17-5

Step 1. Dissolve 4-chloro-3-methoxybenzoic acid (1.12 g, 5.98 mmol) in tetrahydrofuran (30 mL) under ice bath conditions with stirring. A tetrahydrofuran solution of 1.0 M lithium aluminum hydride (7.18 mL, 7.18 mmol) was slowly added over approximately 5 minutes. Ice bath conditions were maintained and stirring of the reaction mixture was continued for 2 hours. Upon completion of the reaction, the reaction was quenched by slow dropwise addition of water (0.27 mL), followed by addition of 15% aqueous sodium hydroxide solution (0.27 mL), and finally water (0.82 mL). The resulting suspension was filtered and the collected solid was washed with ethyl acetate. The filtrates were combined and concentrated under reduced pressure to give (4-chloro-3-methoxyphenyl)methanol as a colorless oil (737 mg, 71% yield). The product was characterized by 1H NMR (400 MHz, CDCl3): δ 3.92 (s, 3H), 4.67 (s, 2H), 6.87 (d, J = 7.6 Hz, 1H), 6.98 (s, 1H), 7.33 (d, J = 7.6 Hz, 1H).

References

[1] Patent: US2002/77486, 2002, A1
[2] Patent: US6906063, 2005, B2
[3] Patent: EP2314593, 2016, B1. Location in patent: Paragraph 0201
[4] Journal of Medicinal Chemistry, 1987, vol. 30, # 10, p. 1887 - 1891
[5] Journal of Medicinal Chemistry, 1992, vol. 35, # 23, p. 4408 - 4414

(4-Chloro-3-Methoxyphenyl)Methanol Preparation Products And Raw materials

Raw materials

Preparation Products

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13726-17-5, (4-Chloro-3-Methoxyphenyl)MethanolRelated Search:

(4-Chloro-3-Methoxyphenyl)Methanol

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13726-17-5