ChemicalBook > CAS DataBase List > 6-Methyl-1H-pyrrolo[2,3-b]pyridine

6-Methyl-1H-pyrrolo[2,3-b]pyridine

Product Name
6-Methyl-1H-pyrrolo[2,3-b]pyridine
CAS No.
824-51-1
Chemical Name
6-Methyl-1H-pyrrolo[2,3-b]pyridine
Synonyms
113877;6-METHYL-7-AZAINDOLE;6-METHYL-1H-PYRROLO[2,3-B]PYRIDINE;1H-Pyrrolo[2,3-b]pyridine, 6-methyl-
CBNumber
CB9267730
Molecular Formula
C8H8N2
Formula Weight
132.16
MOL File
824-51-1.mol
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6-Methyl-1H-pyrrolo[2,3-b]pyridine Property

Melting point:
140℃
Boiling point:
368.4±15.0 °C(Predicted)
Density 
1.17
storage temp. 
2-8°C
form 
White to yellow powder or crystals
pka
7.71±0.40(Predicted)
Appearance
Off-white to light brown Solid
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Safety

HS Code 
2933998090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P310Immediately call a POISON CENTER or doctor/physician.

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N-Bromosuccinimide Price

TRC
Product number
M328430
Product name
6-methyl-1H-pyrrolo[2,3-b]pyridine
Packaging
50mg
Price
$130
Updated
2021/12/16
ChemScene
Product number
CS-B0515
Product name
6-Methyl-1H-pyrrolo[2,3-b]pyridine
Packaging
250mg
Price
$51
Updated
2021/12/16
ChemScene
Product number
CS-B0515
Product name
6-Methyl-1H-pyrrolo[2,3-b]pyridine
Packaging
1g
Price
$107
Updated
2021/12/16
Apolloscientific
Product number
OR929870
Product name
6-Methyl-1H-pyrrolo[2,3-b]pyridine
Purity
98%
Packaging
250mg
Price
$200
Updated
2021/12/16
AK Scientific
Product number
W8621
Product name
6-Methyl-1H-pyrrolo[2,3-b]pyridine
Packaging
1g
Price
$207
Updated
2021/12/16
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6-Methyl-1H-pyrrolo[2,3-b]pyridine Chemical Properties,Usage,Production

Synthesis

823-96-1

55052-27-2

824-51-1

The general procedure for the synthesis of 6-methyl-7-azaindole from trimethylcyclotriboroxane and 6-chloro-1H-pyrrolo[2,3-B]pyridine is as follows: 1. 6-methyl-7-aza-indole (1.00 g, 6.55 mmol), 2,4,6-trimethyl-1,3,5,2,4,6-trioxa-triazine (1.0 ml, 7.2 mmol), and potassium carbonate (2.72 g, 19.7 mmol) were suspended in 13 ml of dimethoxyethane and degassed in a microwave reactor with three vacuum-argon cycles . 2. [1,1'-Bis(diphenylphosphino)ferrocene]-palladium(II) dichloride complex with dichloromethane (0.29 g, 0.33 mmol) was added and again degassed in three vacuum-argon cycles. 3. the reaction mixture was stirred at 120 °C for 2 h under microwave radiation. 4. After completion of the reaction, the mixture was cooled, filtered through diatomaceous earth and eluted with ethyl acetate. 5. The filtrate was concentrated under pressure and the residue was purified by an Isolera purification system (ethyl acetate-hexane gradient, 0:100 ascending to 50:50) to afford 0.57 g (4.31 mmol, 65% yield) of 6-methyl-7-azaindole as a beige solid with 98% purity. Product characterization data: 1H NMR (300 MHz, chloroform-d) δ ppm: 10.87 (br.s., 1H), 7.86 (d, J = 7.63 Hz, 1H), 7.29 (dd, J = 3.52, 2.35 Hz, 1H), 6.97 (d, J = 7.63 Hz, 1H), 6.47 (dd, J = 3.52, 1.76 Hz, 1H) , 2.69 (s, 3H). HPLC/MS (15 min) Retention time: 2.57 min. LRMS: m/z 133 (M + 1).

References

[1] Patent: WO2013/10880, 2013, A1. Location in patent: Page/Page column 104
[2] Patent: EP2548876, 2013, A1. Location in patent: Paragraph 0442-0445

6-Methyl-1H-pyrrolo[2,3-b]pyridine Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 6-Methyl-1H-pyrrolo[2,3-b]pyridine manufacturers

Henan Aochuang Chemical Co.,Ltd.
Product
6-METHYL-1H-PYRROLO[2,3-B]PYRIDINE 824-51-1
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
1Ton
Release date
2022-10-13
Career Henan Chemical Co
Product
6-Methyl-7-azaindole 824-51-1
Price
US $1.00/g
Min. Order
1g
Purity
95--99%
Supply Ability
1ton
Release date
2020-01-09
Career Henan Chemical Co
Product
6-METHYL-1H-PYRROLO[2,3-B]PYRIDINE 824-51-1
Price
US $1.00/g
Min. Order
1g
Purity
99%
Supply Ability
200kg
Release date
2020-01-08

824-51-1, 6-Methyl-1H-pyrrolo[2,3-b]pyridineRelated Search:

6-Chloro-1H-pyrazolo[4,3-c]pyridine N,6-DIMETHYLPYRIDIN-2-AMINE 1H-PYRROLO[2,3-B]PYRIDINE-6-CARBONITRILE 6-TRIFLUOROMETHYL-1H-PYRROLO[2,3-B]PYRIDINE 6-METHYL-1H-PYRROLO[2,3-B]PYRIDINE N-[2-(2,4-DIMETHYL-9H-PYRIDO[2,3-B]INDOL-9-YL)ETHYL]-2-FURAMIDE IMPLITAPIDE N-[2-(2,4-DIMETHYL-9H-PYRIDO[2,3-B]INDOL-9-YL)ETHYL]-1-(4-FLUOROPHENYL)-5-METHYL-1H-1,2,3-TRIAZOLE-4-CARBOXAMIDE 2,4-DIMETHYL-1-AZACARBAZOLE-3-PROPIONIC ACID ETHYL ESTER N-[2-(2,4-DIMETHYL-9H-PYRIDO[2,3-B]INDOL-9-YL)ETHYL]-8-QUINOLINECARBOXAMIDE N-[2-(2,4-DIMETHYL-9H-PYRIDO[2,3-B]INDOL-9-YL)ETHYL]-N'-(4-METHYLPHENYL)THIOUREA 2-CHLORO-N-[2-(2,4-DIMETHYL-9H-PYRIDO[2,3-B]INDOL-9-YL)ETHYL]BENZAMIDE N-(3-CHLOROPHENYL)-N'-[2-(2,4-DIMETHYL-9H-PYRIDO[2,3-B]INDOL-9-YL)ETHYL]THIOUREA N-[2-(2,4-DIMETHYL-9H-PYRIDO[2,3-B]INDOL-9-YL)ETHYL]-3,4,5-TRIMETHOXYBENZAMIDE N-[2-(2,4-DIMETHYL-9H-PYRIDO[2,3-B]INDOL-9-YL)ETHYL]ISONICOTINAMIDE N-[2-(2,4-DIMETHYL-9H-PYRIDO[2,3-B]INDOL-9-YL)ETHYL]-5-METHYL-3-PHENYL-4-ISOXAZOLECARBOXAMIDE 2-(2,4-DIMETHYL-9H-PYRIDO[2,3-B]INDOL-9-YL)ETHANAMINE DIHYDROCHLORIDE N-[2-(2,4-DIMETHYL-9H-PYRIDO[2,3-B]INDOL-9-YL)ETHYL]-3-FLUOROBENZAMIDE

  • 113877
  • 1H-Pyrrolo[2,3-b]pyridine, 6-methyl-
  • 6-METHYL-7-AZAINDOLE
  • 6-METHYL-1H-PYRROLO[2,3-B]PYRIDINE
  • 824-51-1