9-(1-Naphthyl) carbazole
Uses- Product Name
- 9-(1-Naphthyl) carbazole
- CAS No.
- 22034-43-1
- Chemical Name
- 9-(1-Naphthyl) carbazole
- Synonyms
- DYPR0399;9-Napthylcarbazole;9-(1-Naphthyl) carbazole;9-(1-Naphthyl)carbazole>9-naphthalen-1-ylcarbazole;9-(1-naphthalenyl)-9H-Carbazole;9-(naphthalen-1-yl)-9H-carbazole;9H-Carbazole, 9-(1-naphthalenyl)-
- CBNumber
- CB92686654
- Molecular Formula
- C22H15N
- Formula Weight
- 293.36
- MOL File
- 22034-43-1.mol
9-(1-Naphthyl) carbazole Property
- Melting point:
- 126.0 to 131.0 °C
- Boiling point:
- 503.7±23.0 °C(Predicted)
- Density
- 1.15±0.1 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- form
- powder to crystal
- color
- White to Almost white
- λmax
- 321nm(Cyclohexane)(lit.)
- InChI
- InChI=1S/C22H15N/c1-2-10-17-16(8-1)9-7-15-20(17)23-21-13-5-3-11-18(21)19-12-4-6-14-22(19)23/h1-15H
- InChIKey
- QSOAYCUFEQGHDN-UHFFFAOYSA-N
- SMILES
- N1(C2=C3C(C=CC=C3)=CC=C2)C2=C(C=CC=C2)C2=C1C=CC=C2
Safety
- HS Code
- 2933.99.9701
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
N-Bromosuccinimide Price
- Product number
- N1012
- Product name
- 9-(1-Naphthyl)carbazole
- Purity
- >98.0%(GC)
- Packaging
- 1g
- Price
- $152
- Updated
- 2025/07/31
- Product number
- N1012
- Product name
- 9-(1-Naphthyl)carbazole
- Purity
- >98.0%(GC)
- Packaging
- 5g
- Price
- $533
- Updated
- 2025/07/31
- Product number
- N378493
- Product name
- 9-(Naphthalen-1-yl)-9H-carbazole
- Packaging
- 100mg
- Price
- $75
- Updated
- 2021/12/16
- Product number
- 6914AL
- Product name
- 9-(1-Naphthyl)carbazole
- Packaging
- 10g
- Price
- $142
- Updated
- 2021/12/16
- Product number
- 42740
- Product name
- 9-(1-Naphthyl)carbazole,≥98%(GC)
- Purity
- ≥98%(GC)
- Packaging
- 1G
- Price
- $182.58
- Updated
- 2021/12/16
9-(1-Naphthyl) carbazole Chemical Properties,Usage,Production
Uses
9-(Naphthalen-1-yl)-9H-carbazole is a useful research chemical.
Synthesis
90-11-9
86-74-8
22034-43-1
[Example 8]; [0397] In this embodiment, the method for the synthesis of 2-{N-(1-naphthalenyl)-N-[9-(1-naphthalenyl)carbazol-3-yl]amino}-9,10-diphenylanthracene (abbreviation: 2NCNPA) is specifically described by the anthracene derivative of the present invention represented by structural formula (220). ; [Step 1] Synthesis of N,N-diethylnaphthalenyl-H-carbazol-S-amine (abbreviation: NCN) (i) Synthesis of 9-(1-naphthalenyl)carbazole. the scheme for the synthesis of 9-(1-naphthalenyl)carbazole is illustrated in (C-18). 21 g (0.1 mol) of 1-bromonaphthalene, 17 g (0.1 mol) of carbazole, 950 mg (5 mmol) of copper (I) iodide, 33 g (240 mmol) of potassium carbonate, and 660 mg (2.5 mmol) of 18-crown-6-ether were added to a 500 mL three-necked flask with nitrogen displacement. To this mixture was added 80 mL of 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone (abbreviation: DMPU), which was then stirred at 170 °C for 6 h under nitrogen protection. To this reaction mixture was added a further 10 g (50 mmol) of 1-bromonaphthalene, 2.0 g (10 mmol) of copper (I) iodide and 2.6 g (10 mmol) of 18-crown-6-ether and stirring was continued at 170 °C for 7.5 hours. Further 10 g (50 mmol) of 1-bromonaphthalene was added to this reaction mixture and stirring was continued at 180 °C for 6 hours. Upon completion of the reaction, about 200 mL of toluene and about 100 mL of 1 mol/L hydrochloric acid were added to this reaction mixture, and then the mixture was filtered through diatomaceous earth. The resulting filtrate was sequentially filtered through Florisil and diatomaceous earth. The organic and aqueous layers of the resulting filtrate were separated, and the organic layer was washed with 1 mol/L hydrochloric acid, then with water, and finally dried with magnesium sulfate. The suspension was filtered through Florisil and diatomaceous earth. The filtrate was concentrated to give an oil to which methanol was added and sonicated to precipitate solids. The precipitated solid was collected by filtration to give 22 g of 9-(1-naphthyl)carbazole as a white powder (75% yield).The Rf values (SiO2, eluent; hexane:ethyl acetate=10:1) for 9-(1-naphthyl)carbazole, 1-bromonaphthalene, and carbazole were 0.61, 0.74, and 0.24, respectively.
References
[1] Patent: WO2007/125934, 2007, A1. Location in patent: Page/Page column 168-169
[2] Patent: WO2009/72587, 2009, A1. Location in patent: Page/Page column 237-238
[3] Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2006, vol. 63, # 1, p. 15 - 20
[4] Journal of Organic Chemistry, 2009, vol. 74, # 9, p. 3341 - 3349
9-(1-Naphthyl) carbazole Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 9-(1-Naphthyl) carbazole manufacturers
- Product
- 9-(1-Naphthyl) carbazole 22034-43-1
- Price
- US $0.00/kg
- Min. Order
- 1kg
- Purity
- 99%
- Supply Ability
- 10000KGS
- Release date
- 2025-12-02
- Product
- 9-(1-naphthyl)carbazole 22034-43-1
- Price
- US $0.00-0.00/kg
- Min. Order
- 1kg
- Purity
- 99%min
- Supply Ability
- 10 tons
- Release date
- 2025-08-18
- Product
- 9-(1-Naphthyl) carbazole 22034-43-1
- Price
- US $200.00-1.00/KG
- Min. Order
- 1KG
- Purity
- 99%, 99.5% Sublimated
- Supply Ability
- g-kg-tons, free sample is available
- Release date
- 2023-12-30