3-(6-BroMopyridin-3-yl)acrylic acid
- Product Name
- 3-(6-BroMopyridin-3-yl)acrylic acid
- CAS No.
- 1035123-89-7
- Chemical Name
- 3-(6-BroMopyridin-3-yl)acrylic acid
- Synonyms
- 3-(6-Bromopyridin-3-yl);3-(6-BroMopyridin-3-yl)acrylic acid;(2E)-3-(6-Bromo-3-pyridinyl)acrylic acid;3-(6-BroMopyridin-3-yl)prop-2-enoic acid;3-(6-bromo-3-pyridinyl)-2-Propenoic acid;(Z/E)-3-(6-bromopyridin-3-yl)acrylic acid;2-Propenoic acid, 3-(6-bromo-3-pyridinyl)-
- CBNumber
- CB92723371
- Molecular Formula
- C8H6BrNO2
- Formula Weight
- 228.04
- MOL File
- 1035123-89-7.mol
3-(6-BroMopyridin-3-yl)acrylic acid Property
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- HCH0364262
- Product name
- 3-(6-BROMOPYRIDIN-3-YL)ACRYLIC ACID
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $496.96
- Updated
- 2021/12/16
- Product number
- 6565941
- Product name
- 3-(6-Bromopyridin-3-yl)acrylicacid
- Purity
- 95%
- Packaging
- 5G
- Price
- $950
- Updated
- 2021/12/16
- Product number
- CM174673
- Product name
- (E)-3-(6-bromopyridin-3-yl)acrylicacid
- Purity
- 98%
- Packaging
- 5g
- Price
- $1108
- Updated
- 2021/12/16
- Product number
- 1035123897
- Product name
- 3-(6-Bromopyridin-3-yl)acrylicacid
- Packaging
- 5g
- Price
- $1149.45
- Updated
- 2021/12/16
- Product number
- CM174673
- Product name
- (E)-3-(6-bromopyridin-3-yl)acrylicacid
- Purity
- 98%
- Packaging
- 10g
- Price
- $1648
- Updated
- 2021/12/16
3-(6-BroMopyridin-3-yl)acrylic acid Chemical Properties,Usage,Production
Synthesis
918305-33-6
1035123-89-7
Step 2: Synthesis of 3-(6-bromopyridin-3-yl)acrylic acid To a tetrahydrofuran (THF) solution of methyl 3-(6-bromopyridin-3-yl)acrylate (120 mg, 0.495 mmol) was added an aqueous 0.5 N lithium hydroxide (LiOH) solution (2 equiv). The reaction mixture was stirred at room temperature for 3 hours. After completion of the reaction, the resulting residue was dissolved in water (H2O) and washed three times with ether (Et2O). Subsequently, it was neutralized with 1 N hydrochloric acid (HCl) to pH 5~7. The resulting solid was collected by filtration, washed with water and dried under vacuum to afford 3-(6-bromopyridin-3-yl)acrylic acid (100 mg, 88% yield). 1H NMR (300 MHz, DMSO-d6): δ 8.67 (d, 1H, J = 2.1 Hz), 8.11 (dd, 1H, J = 8.4, 2.1 Hz), 7.69 (d, 1H, J = 8.4 Hz), 7.59 (d, 1H, J = 15.9 Hz), 6.71 (d, 1H, J = 15.9 Hz).
References
[1] Patent: EP1882687, 2008, A1. Location in patent: Page/Page column 27
3-(6-BroMopyridin-3-yl)acrylic acid Preparation Products And Raw materials
Raw materials
Preparation Products
3-(6-BroMopyridin-3-yl)acrylic acid Suppliers
- Tel
- 0531-81313138 13066006660
- Fax
- QQ: 3366077777
- chibapharm@foxmail.com
- Country
- China
- ProdList
- 3989
- Advantage
- 55
- Tel
- 400-400-164-7117 18317119277
- Fax
- +86-21-61629029
- product02@bidepharm.com
- Country
- China
- ProdList
- 39999
- Advantage
- 60
- Tel
- 021-18721936-595 18721936595
- Fax
- -
- shkylpharma@126.com
- Country
- China
- ProdList
- 748
- Advantage
- 55
- Tel
- 021-60546673 13701861782
- Fax
- QQ:670259431
- kuanga111@sina.com
- Country
- China
- ProdList
- 925
- Advantage
- 58
- Tel
- 0-2022843681 15618226720
- Fax
- +86-21-51601218
- chaolaichem@foxmail.com
- Country
- China
- ProdList
- 9955
- Advantage
- 58
- Tel
- 0371-0371-55629727 13323845623
- Fax
- 037155629727
- 2885676761@qq.com
- Country
- China
- ProdList
- 10026
- Advantage
- 58
- Tel
- 571-89925085
- Fax
- 0086-571-89925065
- sales@amadischem.com
- Country
- China
- ProdList
- 131957
- Advantage
- 58
- Tel
- 13356901049
- Fax
- QQ：1025383091
- 3119594100@qq.com
- Country
- China
- ProdList
- 7964
- Advantage
- 55
- Tel
- 13127280945
- 285424065@qq.com
- Country
- China
- ProdList
- 9976
- Advantage
- 55
- Tel
- 025-66113011 19370895928
- Fax
- (7)02557626880
- qzhang@aikonchem.com
- Country
- China
- ProdList
- 15393
- Advantage
- 58
View Lastest Price from 3-(6-BroMopyridin-3-yl)acrylic acid manufacturers
- Product
- (2E)-3-(6-Bromo-3-pyridinyl)acrylic acid 1035123-89-7
- Price
- US $1.00/GK
- Min. Order
- 1g
- Purity
- Min98% HPLC
- Supply Ability
- g/kg/ton
- Release date
- 2020-02-07