6-BroMoquinoline-3-carboxaMide
- Product Name
- 6-BroMoquinoline-3-carboxaMide
- CAS No.
- 1296950-96-3
- Chemical Name
- 6-BroMoquinoline-3-carboxaMide
- Synonyms
- 6-BroMoquinoline-3-carboxaMide;3-Quinolinecarboxamide, 6-bromo-
- CBNumber
- CB92735888
- Molecular Formula
- C10H7BrN2O
- Formula Weight
- 251.08
- MOL File
- 1296950-96-3.mol
6-BroMoquinoline-3-carboxaMide Property
- Boiling point:
- 471.9±25.0 °C(Predicted)
- Density
- 1.655±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 14.85±0.30(Predicted)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- CD11298480
- Product name
- 6-Bromoquinoline-3-carboxamide
- Purity
- 97%
- Packaging
- 250mg
- Price
- $244
- Updated
- 2021/12/16
- Product number
- CM142965
- Product name
- 6-bromoquinoline-3-carboxamide
- Purity
- 97%
- Packaging
- 1g
- Price
- $574
- Updated
- 2021/12/16
- Product number
- CD11298480
- Product name
- 6-Bromoquinoline-3-carboxamide
- Purity
- 97%
- Packaging
- 1g
- Price
- $608
- Updated
- 2021/12/16
- Product number
- 1296950963
- Product name
- 6-Bromoquinoline-3-carboxamide
- Packaging
- 1g
- Price
- $646.8
- Updated
- 2021/12/16
- Product number
- CM142965
- Product name
- 6-bromoquinoline-3-carboxamide
- Purity
- 97%
- Packaging
- 5g
- Price
- $1427
- Updated
- 2021/12/16
6-BroMoquinoline-3-carboxaMide Chemical Properties,Usage,Production
Synthesis
798545-30-9
1296950-96-3
General procedure for the synthesis of 6-bromoquinoline-3-carboxamide from 6-bromoquinoline-3-carboxylic acid: Step 1: To a suspension of 6-bromoquinoline-3-carboxylic acid (0.50 g, 1.98 mmol) in dichloromethane (10 ml) was slowly added oxalyl chloride (327 mg, 0.22 ml, 2.58 mmol) followed by dropwise addition of DMF (3 drops). Mild gas escape was observed during the reaction. The reaction mixture was stirred at room temperature for 2 h and subsequently concentrated by rotary evaporation to give a white solid. The residue was resuspended in ether (10 ml) and 28% aqueous ammonium hydroxide solution (2.0 ml, 16.0 mmol) was slowly added. The mixture was stirred vigorously at room temperature for 2 h. After completion of the reaction, the precipitate was collected by filtration and washed sequentially with water and ether. The product was dried under high vacuum to give 457 mg (92% yield) of 6-bromoquinoline-3-carboxamide as a beige solid.
References
[1] Patent: WO2014/86697, 2014, A1. Location in patent: Page/Page column 44-45
6-BroMoquinoline-3-carboxaMide Preparation Products And Raw materials
Raw materials
Preparation Products
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