9,9-Diphenylfluorene-2-Boronic acid pinacol ester

Product Name: 9,9-Diphenylfluorene-2-Boronic acid pinacol ester
CAS No.: 462128-39-8
Chemical Name: 9,9-Diphenylfluorene-2-Boronic acid pinacol ester
Synonyms: diphenylfluorene;uoren-2-yL;2-(9,9-DiphenyL;9,9-Diphenylfluoren-2-borate pinacol ester;9,9-Diphenylfluorene-2-Boronic acid picol ester;9,9-Diphenylfluorene-2-Boronic acid pinacol ester;9,9-Diphenyl-9H-fluoren-2-ylboronic acid pinacol ester;(1,5-Cyclooctadiene)(pyridine)(tricyclohexylphosphine);2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)-9,9-diphenylfluorene;9,9-Diphenylfluorene-2-Boronic acid pinacol ester ISO 9001：2015 REACH
CBNumber: CB92737589
Molecular Formula: C31H29BO2
Formula Weight: 444.37
MOL File: 462128-39-8.mol

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9,9-Diphenylfluorene-2-Boronic acid pinacol ester Property

Melting point:: 198.0 to 202.0 °C
Boiling point:: 556.2±29.0 °C(Predicted)
Density: 1.17±0.1 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
form: powder to crystal
color: White to Almost white

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Safety

HS Code: 2934.99.4400

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TCI Chemical

Product number: D5009
Product name: 2-(9,9-Diphenyl-9H-fluoren-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
Purity: >97.0%(HPLC)(T)
Packaging: 200mg
Price: $45
Updated: 2025/07/31

TCI Chemical

Product number: D5009
Product name: 2-(9,9-Diphenyl-9H-fluoren-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
Purity: >97.0%(HPLC)(T)
Packaging: 1g
Price: $132
Updated: 2025/07/31

TRC

Product number: D493993
Product name: 2-(9,9-Diphenyl-9H-fluoren-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
Packaging: 25mg
Price: $75
Updated: 2021/12/16

AK Scientific

Product number: 9599AL
Product name: 2-(9,9-Diphenyl-9H-fluoren-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
Packaging: 250mg
Price: $72
Updated: 2021/12/16

AK Scientific

Product number: 9599AL
Product name: 2-(9,9-Diphenyl-9H-fluoren-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
Packaging: 5g
Price: $157
Updated: 2021/12/16

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9,9-Diphenylfluorene-2-Boronic acid pinacol ester Chemical Properties,Usage,Production

Synthesis

73183-34-3

474918-32-6

462128-39-8

The general procedure for the synthesis of 2-(9,9-diphenyl-9H-fluoren-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane from biphenylpinacol ester and 2-bromo-9,9-diphenylfluorene was carried out in the following manner: in a single-necked round-bottomed flask, 2-bromo-9,9-diphenyl-9H-fluorene (40 g, 100.67 mmol), biphenylpinacol ester (51.1 g, 201.34 mmol), PdCl2(dppf) (2.2 g, 3.02 mmol), KOAc (29.6 g, 302.01 mmol) and DMF (400 ml) were mixed and the reaction was carried out at reflux. Upon completion of the reaction, the mixture was extracted with dichloromethane and the organic phase was dried with anhydrous MgSO4, followed by removal of the solvent DMF under reduced pressure by rotary evaporator.The crude product was purified by column chromatography (silica gel as stationary phase, eluent hexane and dichloromethane in a 1:1 ratio, v/v/v/v) to afford the white solid product 2-(9,9-diphenyl-9H-fluoren-2-yl)-4,4,5,5-tetramethyl- 1,3,2-dioxaborolane (41 g, 91% yield).

References

[1] Patent: CN105408333, 2016, A. Location in patent: Paragraph 0212; 0213; 0214

9,9-Diphenylfluorene-2-Boronic acid pinacol ester Preparation Products And Raw materials

Raw materials

Preparation Products

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9,9-Diphenylfluorene-2-Boronic acid pinacol ester Suppliers

Americas 1 CHINA 88 Europe 1 India 2 Japan 1 United States 3 Global 96

TCI AMERICA

Tel: 800-4238616
Fax: +1-888-520-1075 / +1-503-283-1987
Email: sales@tciamerica.com
Country: Americas
ProdList: 23653
Advantage: 75

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View Lastest Price from 9,9-Diphenylfluorene-2-Boronic acid pinacol ester manufacturers

Henan Aochuang Chemical Co.,Ltd.

Product: 9,9-Diphenylfluorene-2-Boronic acid pinacol ester 462128-39-8
Price: US $5.00/kg
Min. Order: 1kg
Purity: 97%
Supply Ability: 100kg
Release date: 2025-04-01

Shanghai Daken Advanced Materials Co.,Ltd

Product: 9,9-Diphenylfluorene-2-Boronic acid pinacol ester 462128-39-8
Price: US $0.00/KG
Min. Order: 1KG
Purity: 98.00%
Supply Ability: 150KG /month
Release date: 2021-11-12

Henan Fengda Chemical Co., Ltd

Product: 9,9-Diphenylfluorene-2-Boronic acid pinacol ester 462128-39-8
Price: US $200.00-1.00/KG
Min. Order: 1KG
Purity: 99%, 99.5% Sublimated
Supply Ability: g-kg-tons, free sample is available
Release date: 2024-01-02

462128-39-8, 9,9-Diphenylfluorene-2-Boronic acid pinacol esterRelated Search:

2-(9H-Fluoren-2-yl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane 1,3,2-DIOXABOROLANE, 2-(9,9-DIMETHYL-9H-FLUOREN-2-YL)-4,4,5,5-TETRAMETHYL 9,9'-spirobi[fluorene]-2,2'-diyldiboronic acid (2,7-BIS(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-9,9-DIOCTYLFLUORENE) 9,9-DiMethylfluorene-3-boronic acid pinacol ester 4,4,5,5-tetramethyl-2-(9,9'-spirobi[9H-fluoren]-4-yl)-1,3,2-Dioxaborolane 9,9-Spirodifluorene-2-Boronic acid pinacol ester 4 - boric acid pinacol ester - 9, 9 - dimethyl fluorene 9,9-Spirodifluorene-3-Boronic acid pinacol ester 9,9-diphenyl-9H-fluoreN-4-ylboronicacid 4-Pinacol ester-9,9-dipehnylfluorene 1,3,2-DIOXABOROLANE, 2,2'-(9,9-DIMETHYL-9H-FLUORENE-2,7-DIYL)BIS[4,4,5,5-TETRAMETHYL] 9,9-diphenyl-fluoren-3-boronic acid pinacol ester

9,9-Diphenylfluorene-2-Boronic acid pinacol ester

2-(9,9-Diphenyl-9H-fluoren-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

9,9-Diphenyl-9H-fluoren-2-ylboronic acid pinacol ester

2-(9,9-Diphenyl-9<i>H</i>-fluoren-2-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

9,9-Diphenylfluorene-2-Boronic acid picol ester

2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)-9,9-diphenylfluorene

diphenylfluorene

2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9,9-diphenyl-9H-fluorene

2-(9,9-DiphenyL

uoren-2-yL

1,3,2-Dioxaborolane, 2-(9,9-diphenyl-9H-fluoren-2-yl)-4,4,5,5-tetramethyl-

9,9-Diphenyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-fluorene

9,9-Diphenylfluorene-2-Boronic acid pinacol ester ISO 9001：2015 REACH

2-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolane-2-yl)-9,9-diphenyl-9H-fluoren

9,9-Diphenylfluoren-2-borate pinacol ester

(1,5-Cyclooctadiene)(pyridine)(tricyclohexylphosphine)

462128-39-8

C31H29BO2