2-BROMO-5-CHLORO-4-METHYL-ANILINE

Product Name: 2-BROMO-5-CHLORO-4-METHYL-ANILINE
CAS No.: 102170-52-5
Chemical Name: 2-BROMO-5-CHLORO-4-METHYL-ANILINE
Synonyms: 4-Amino-5-bromo-2-chlorotoluene;2-chloro-5-bromo-4-aminotoluene;2-BROMO-5-CHLORO-4-METHYL-ANILINE;2-bromo-5-chloro-4-methylbenzenamine;2-Bromo-5-chloro-4-methyl-phenylamine;Benzenamine, 2-bromo-5-chloro-4-methyl-
CBNumber: CB9300176
Molecular Formula: C7H7BrClN
Formula Weight: 220.49
MOL File: 102170-52-5.mol

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2-BROMO-5-CHLORO-4-METHYL-ANILINE Property

Melting point:: 90 °C
Boiling point:: 281.3±35.0 °C(Predicted)
Density: 1.619±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 1.91±0.10(Predicted)
Appearance: White to off-white Solid
InChI: InChI=1S/C7H7BrClN/c1-4-2-5(8)7(10)3-6(4)9/h2-3H,10H2,1H3
InChIKey: ULCBEYQOSOVMMA-UHFFFAOYSA-N
SMILES: C1(N)=CC(Cl)=C(C)C=C1Br

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Safety

Hazard Codes: Xi
HS Code: 2921420090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B821088
Product name: 2-Bromo-5-chloro-4-methylaniline
Packaging: 50mg
Price: $60
Updated: 2021/12/16

AK Scientific

Product number: X8594
Product name: 2-Bromo-5-chloro-4-methylaniline
Packaging: 1g
Price: $145
Updated: 2021/12/16

Apolloscientific

Product number: OR59373
Product name: 2-Bromo-5-chloro-4-methylaniline
Packaging: 1g
Price: $163
Updated: 2021/12/16

SynQuest Laboratories

Product number: 3730-D-07
Product name: 2-Bromo-5-chloro-4-methylaniline
Packaging: 1g
Price: $192
Updated: 2021/12/16

Matrix Scientific

Product number: 140132
Product name: 2-Bromo-5-chloro-4-methylaniline
Purity: 95%+
Packaging: 5g
Price: $366
Updated: 2021/12/16

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2-BROMO-5-CHLORO-4-METHYL-ANILINE Chemical Properties,Usage,Production

Synthesis

95-74-9

102170-52-5

Example 4: (5-Chloro-2-((E)-3-(3-(4-fluorophenyl)-3,8-diazanaphthalen-1-yl)-3-oxopropenyl)-4-methylphenyl)urea; a) Synthesis of 2-bromo-5-chloro-4-methylaniline; 3-chloro-4-methylaniline (20.0 g, 0.141 mol) was dissolved in dichloromethane (200 mL) and a 5 minute A solution of N-bromosuccinimide (NBS, 25.1 g, 0.141 mol) in dichloromethane (800 mL) was added slowly over 5 min. The reaction mixture was stirred at room temperature for 5 minutes. Subsequently, the reaction solution was concentrated to about 200 mL and diluted with hexane (1000 mL). The precipitate was collected by filtration, and the filtrate was concentrated and dried and purified by silica gel column chromatography (eluent: hexane/tert-butyl methyl ether, 10:1) to afford the title compound as yellow crystals (12.3 g, 40% yield). A second title compound (7.5 g, 24% yield) was obtained by re-chromatographing the mixed grades.1H-NMR (400 MHz, DMSO-d6) δ (ppm): 2.13 (s, 3H); 5.32 (s, 2H, NH2); 6.81 (s, 1H); 7.31 (s, 1H). Mass spectra (m/z) ES+: 221 (100, [M]+); 219 (80); 184 (35); 140 (100); 104 (50); 77 (65); 52 (58); 51 (60).

References

[1] Patent: WO2005/103054, 2005, A2. Location in patent: Page/Page column 71
[2] Journal of Medicinal Chemistry, 2002, vol. 45, # 17, p. 3692 - 3702

2-BROMO-5-CHLORO-4-METHYL-ANILINE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-BROMO-5-CHLORO-4-METHYL-ANILINE Suppliers

China 49 India 1 United Kingdom 2 United States 12 Global 64

Shanghai Zhixia Chemical Technology Co., LTD

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Jiangsu Aikon Biopharmaceutical R&D co.,Ltd.

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9ding chemical ( Shanghai) Limited

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Bide Pharmatech Ltd.

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View Lastest Price from 2-BROMO-5-CHLORO-4-METHYL-ANILINE manufacturers

ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD

Product: 2-Bromo-5-chloro-4-methylaniline 102170-52-5
Price: US $3.00-9.00/KG
Min. Order: 0.1KG
Purity: 99%
Supply Ability: g-kg-tons, free sample is available
Release date: 2025-06-26

102170-52-5, 2-BROMO-5-CHLORO-4-METHYL-ANILINERelated Search:

5-BROMO-2-CHLOROTOLUENE 2-Chlorotoluene 4-Bromo-3-chloro-2-methylaniline 4-Bromo-2-chloro-6-methylaniline 4-(1,3-BENZOTHIAZOL-2-YL)-2,6-DIBROMO-3-CHLOROANILINE 2,6-DIBROMO-3-CHLORO-4-[1,3]OXAZOLO[4,5-B]PYRIDIN-2-YLANILINE 2-BROMO-5-CHLORO-4-METHYL-ANILINE 3-CHLORO-2,6-DIBROMO-4-METHYLANILINE 3-Chloro-2,6-dibromo-4-methylphenylisothiocyanate N-(2,6-DIBROMO-3-CHLORO-4-METHYLPHENYL)OXO(DIPHENYL)PHOSPHORANECARBOTHIOAMIDE

2-BROMO-5-CHLORO-4-METHYL-ANILINE

2-Bromo-5-chloro-4-methyl-phenylamine

4-Amino-5-bromo-2-chlorotoluene

Benzenamine, 2-bromo-5-chloro-4-methyl-

2-bromo-5-chloro-4-methylbenzenamine

2-chloro-5-bromo-4-aminotoluene

102170-52-5

Amines

blocks

Bromides