tert-butyl N-methoxycarbamate

Product Name: tert-butyl N-methoxycarbamate
CAS No.: 58377-44-9
Chemical Name: tert-butyl N-methoxycarbamate
Synonyms: N-Boc-O-methylhydroxylamine;tert-Butyl methoxycarbamate;tert-butyl N-methoxycarbamate;Carbamic acid, N-methoxy-, 1,1-dimethylethyl ester
CBNumber: CB93060637
Molecular Formula: C6H13NO3
Formula Weight: 147.17
MOL File: 58377-44-9.mol

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tert-butyl N-methoxycarbamate Property

Boiling point:: 83-84 °C(Press: 10 Torr)
Density: 1.006±0.06 g/cm3(Predicted)
storage temp.: Storage temp. 2-8°C
Appearance: Colorless to light yellow Liquid

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P321Specific treatment (see … on this label).

P330Rinse mouth.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: B657050
Product name: N-Boc-O-methylHydroxylamine
Packaging: 1g
Price: $165
Updated: 2021/12/16

Matrix Scientific

Product number: 179522
Product name: tert-Butyl N-methoxycarbamate
Packaging: 1g
Price: $248
Updated: 2021/12/16

Matrix Scientific

Product number: 179522
Product name: tert-Butyl N-methoxycarbamate
Packaging: 5g
Price: $743
Updated: 2021/12/16

Crysdot

Product number: CD13010079
Product name: tert-Butylmethoxycarbamate
Purity: 95+%
Packaging: 10g
Price: $357
Updated: 2021/12/16

Acrotein

Product number: AS00419
Product name: N-Boc-O-methylhydroxylamine
Purity: 97%
Packaging: 10g
Price: $366.67
Updated: 2021/12/16

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tert-butyl N-methoxycarbamate Chemical Properties,Usage,Production

Uses

N-Boc-O-methyl Hydroxylamine is used to prepare (pyridinylmethylamino)furanones as insecticides.

Synthesis

24424-99-5

593-56-6

58377-44-9

Example 20: General procedure for the synthesis of tert-butyl methoxycarbamate from di-tert-butyl dicarbonate and methoxyamine hydrochloride Step A: Boc-protected amine (12.0 g, 55.0 mmol) was dissolved in dichloromethane (100 mL) and aqueous sodium carbonate solution (17.5 g sodium carbonate dissolved in 100 mL of water) was added. The reaction mixture was stirred at room temperature for 18 hours. After completion of the reaction, the organic layer was separated, washed with water, dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give a clear oily product (7.94 g, 98% yield).

References

[1] Patent: WO2008/42928, 2008, A2. Location in patent: Page/Page column 48-49
[2] Patent: WO2008/42928, 2008, A2. Location in patent: Page/Page column 48-49
[3] Journal of Organic Chemistry, 1989, vol. 54, # 14, p. 3394 - 3403
[4] Organic and Biomolecular Chemistry, 2012, vol. 10, # 17, p. 3519 - 3530

tert-butyl N-methoxycarbamate Preparation Products And Raw materials

Raw materials

Preparation Products

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tert-butyl N-methoxycarbamate Suppliers

China 30 Germany 1 India 1 United States 5 Global 37

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58377-44-9