BIS (P-DIMETHYLSILYL) PHENYL ETHER

Product Name: BIS (P-DIMETHYLSILYL) PHENYL ETHER
CAS No.: 13315-17-8
Chemical Name: BIS (P-DIMETHYLSILYL) PHENYL ETHER
Synonyms: DK515;SIB 1090;DKFELEX0124;4,4'-Bis(di;Bisdimethylsilylphenylether;BIS (P-DIMETHYLSILYL) PHENYL ETHER;Bis-[(4-dimethylsilyl)-phenyl]-ether;1,1'-Oxybis[4-(dimethylsilyl)benzene;4,4'-Bis(dimethylsilyl)diphenyl ether;Benzene,1,1'-oxybis[4-(diMethylsilyl)-
CBNumber: CB9327207
Molecular Formula: C16H22OSi2
Formula Weight: 286.52
MOL File: 13315-17-8.mol

More

Less

BIS (P-DIMETHYLSILYL) PHENYL ETHER Property

Melting point:: <25°C
Boiling point:: 138 °C
Density: 0.976
refractive index: 1.5478
Flash point:: >110°C
storage temp.: Inert atmosphere,Room Temperature
Specific Gravity: 0.976
Appearance: Colorless to light yellow Liquid
Hydrolytic Sensitivity: 3: reacts with aqueous base
InChI: InChI=1S/C16H22OSi2/c1-18(2)15-9-5-13(6-10-15)17-14-7-11-16(12-8-14)19(3)4/h5-12,18-19H,1-4H3
InChIKey: LMGVLQCDVJCSSQ-UHFFFAOYSA-N
SMILES: O(C1=CC=C([SiH](C)C)C=C1)C1=CC=C([SiH](C)C)C=C1

More

Less

Safety

Risk Statements: 36/37/38
Safety Statements: 26-36/37/39
TSCA: No
HS Code: 29319090

More

Less

Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

More

Less

N-Bromosuccinimide Price

American Custom Chemicals Corporation

Product number: ORS0005396
Product name: BIS (PARA-DIMETHYLSILYL) PHENYL ETHER
Purity: 95.00%
Packaging: 5G
Price: $235.2
Updated: 2021/12/16

AK Scientific

Product number: 3170AL
Product name: Bis[(p-dimethylsilyl)phenyl]ether
Packaging: 25g
Price: $713
Updated: 2021/12/16

Ambeed

Product number: A448209
Product name: (Oxybis(4,1-phenylene))bis(dimethylsilane)
Purity: 97%
Packaging: 25g
Price: $275
Updated: 2021/12/16

Ambeed

Product number: A448209
Product name: (Oxybis(4,1-phenylene))bis(dimethylsilane)
Purity: 97%
Packaging: 250mg
Price: $8
Updated: 2021/12/16

Ambeed

Product number: A448209
Product name: (Oxybis(4,1-phenylene))bis(dimethylsilane)
Purity: 97%
Packaging: 1g
Price: $16
Updated: 2021/12/16

More

Less

BIS (P-DIMETHYLSILYL) PHENYL ETHER Chemical Properties,Usage,Production

Synthesis

31353-78-3

1637-65-6

13315-17-8

The general procedure for the synthesis of bis(4-dimethylsilyl)phenyl ether from the compound (CAS: 31353-78-3) and p-bromophenyl dimethylhydrosilane was as follows: p-bromophenyl dimethylhydrosilane (10.0 g, 46.5 mmol), copper iodide (44.3 mg, 0.233 mmol) and benzotriazole (55.4 mg, 0.465 mmol), followed by the addition of dimethyl sulfoxide (50 mL, 5 mL/g). The mixture was stirred at room temperature for 30 min, then 4-dimethylsilanol (8.50 g, 55.8 mmol) and sodium tert-butoxide (6.26 g, 65.1 mmol) were added. The reaction mixture was stirred at 95-100 °C for 18 hours. After completion of the reaction, water and ethyl acetate were added for extraction, the organic phase was washed with brine, dried over anhydrous sodium sulfate, filtered and concentrated. The reaction mixture was analyzed by HPLC to determine the ratio of impurities A and B as well as the content of target compounds, and the results are shown in Table 2. Finally, the reaction mixture was further purified by fast column chromatography (petroleum ether:dichloromethane = 5:1) and structurally characterized by 1H-NMR.

References

[1] Patent: KR2015/47298, 2015, A. Location in patent: Paragraph 0097; 0104-0105

BIS (P-DIMETHYLSILYL) PHENYL ETHER Preparation Products And Raw materials

Raw materials

Preparation Products

More

Less

BIS (P-DIMETHYLSILYL) PHENYL ETHER Suppliers

China 68 Germany 1 India 1 Singapore 1 United Kingdom 2 United States 6 Global 79

Xuzhou ZhuoYun New Material Technology Co., Ltd.

Tel: 0516-0516 13776763863
Fax: -
Email: zhangqinli.ok@163.com
Country: China
ProdList: 1265
Advantage: 58

J & K SCIENTIFIC LTD.

Tel: 18210857532; 18210857532
Fax: 86-10-82849933
Email: jkinfo@jkchemical.com
Country: China
ProdList: 96815
Advantage: 76

Meryer (Shanghai) Chemical Technology Co., Ltd.

Tel: 4006356688 18621169109
Fax: 86-21-61259102
Email: market03@meryer.com
Country: China
ProdList: 40228
Advantage: 62

Nanjing Chemlin Chemical Co., Ltd

Tel: 025-83697070
Fax: +86-25-83453306
Email: info@chemlin.com.cn
Country: China
ProdList: 15883
Advantage: 64

Shandong Xiya Chemical Co., Ltd

Tel: 4009903999 13355009207
Fax: 0539-6365991
Email: 3007715519@qq.com
Country: China
ProdList: 18729
Advantage: 57

Novel Chemical

Tel: +86-21-64855560, 4008207808
Fax: +86-21-64855560-8021
Email: sales@novelglobal.com
Country: China
ProdList: 124
Advantage: 62

Shanghai chuqing Organosilane technology ltd

Tel: 021-61530618; 18721685818
Fax: 86-21-51714575
Email: sales@chuqingtech.com
Country: China
ProdList: 274
Advantage: 55

Shanghai MOF Chemical Tech Limited

Tel: 13661494087 18964793018
Fax: 86-021-51821718 QQ：2427604606
Email: sales@mof-chemicals.com
Country: China
ProdList: 293
Advantage: 55

Shanghai Gileader Advanced Material Technology Co.,Ltd

Tel: 18516111942
Email: 823898732@qq.com
Country: China
ProdList: 1328
Advantage: 56

Shanghai Worldyang Chemical Co.,Ltd.

Tel: 021-021-56795766
Fax: +86-21-56795266
Email: sales@worldyachem.com
Country: China
ProdList: 9476
Advantage: 58

More

Less

View Lastest Price from BIS (P-DIMETHYLSILYL) PHENYL ETHER manufacturers

Career Henan Chemical Co

Product: BIS (P-DIMETHYLSILYL) PHENYL ETHER 13315-17-8
Price: US $1.00/g
Min. Order: 1g
Purity: 99%
Supply Ability: 200kg
Release date: 2020-01-08

13315-17-8, BIS (P-DIMETHYLSILYL) PHENYL ETHERRelated Search:

BIS (P-DIMETHYLSILYL) PHENYL ETHER 4,4'-Bis(dimethylhydroxysilyl)diphenyl ether BIS-PEG-18 METHYL ETHER DIMETHYL SILANE

BIS (P-DIMETHYLSILYL) PHENYL ETHER

Bisdimethylsilylphenylether

Bis-[(4-dimethylsilyl)-phenyl]-ether

Oxybis(4,1-phenylene)bis(dimethylsilane)

Benzene,1,1'-oxybis[4-(diMethylsilyl)-

SIB 1090

4,4'-Bis(dimethylsilyl)diphenyl ether

4,4'-Bis(di

1,1'-Oxybis[4-(dimethylsilyl)benzene

DK515

DKFELEX0124

13315-17-8