1,3-Dimethylimidazolidin-2-imine hydrochloride
- Product Name
- 1,3-Dimethylimidazolidin-2-imine hydrochloride
- CAS No.
- 87954-60-7
- Chemical Name
- 1,3-Dimethylimidazolidin-2-imine hydrochloride
- Synonyms
- 1,3-Dimethylimidazolidin-2-imine hydrochloride
- CBNumber
- CB93354013
- Molecular Formula
- C5H12ClN3
- Formula Weight
- 149.62188
- MOL File
- 87954-60-7.mol
1,3-Dimethylimidazolidin-2-imine hydrochloride Property
- storage temp.
- Inert atmosphere,Room Temperature
- Appearance
- White to off-white Solid
N-Bromosuccinimide Price
- Product number
- 7743EJ
- Product name
- 1,3-Dimethylimidazolidin-2-iminehydrochloride
- Packaging
- 5g
- Price
- $1103
- Updated
- 2021/12/16
- Product number
- CD00001057
- Product name
- 1,3-Dimethylimidazolidin-2-iminehydrochloride
- Purity
- 97%
- Packaging
- 10g
- Price
- $1171
- Updated
- 2021/12/16
- Product number
- 87954607
- Product name
- 1,3-Dimethylimidazolidin-2-iminehydrochloride
- Packaging
- 10g
- Price
- $1215.4
- Updated
- 2021/12/16
- Product number
- A391142
- Product name
- 1,3-Dimethylimidazolidin-2-iminehydrochloride
- Purity
- 97%
- Packaging
- 100mg
- Price
- $17
- Updated
- 2021/12/16
- Product number
- A391142
- Product name
- 1,3-Dimethylimidazolidin-2-iminehydrochloride
- Purity
- 97%
- Packaging
- 250mg
- Price
- $32
- Updated
- 2021/12/16
1,3-Dimethylimidazolidin-2-imine hydrochloride Chemical Properties,Usage,Production
Synthesis
80-73-9
87954-60-7
The general procedure for the synthesis of 1,3-dimethylimidazolidine-2-imine hydrochloride from 1,3-dimethyl-2-imidazolidinone was as follows: a mixture of 1,3-dimethyl-2-imidazolidinone (20.7 g, 0.18 mol) with triphosgene (15.14 g, 0.051 mol) in 50 mL of carbon tetrachloride was stirred for 5 hours at room temperature. Upon completion of the reaction, the precipitate was collected by filtration, washed with hexane and subsequently dried under vacuum. Ammonia (5 mL) was added to the resulting product in two portions at -50°C until the ammonia was completely evaporated. The final product was obtained as 4.4 g in 12% yield. The results of elemental analysis were as follows (calculated values correspond to C5H13N3Cl-NH4Cl, molecular weight 204.12): C, 29.42%; H, 8.39%; N, 27.45%; Cl, 34.74%. Measured values: C, 28.98%; H, 9.28%; N, 27.74%; Cl, 35.40%.
References
[1] Polyhedron, 2016, vol. 106, p. 75 - 83
1,3-Dimethylimidazolidin-2-imine hydrochloride Preparation Products And Raw materials
Raw materials
Preparation Products
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