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6-bromo-2,3-dihydrobenzofuran-3-ol

Product Name
6-bromo-2,3-dihydrobenzofuran-3-ol
CAS No.
1392072-52-4
Chemical Name
6-bromo-2,3-dihydrobenzofuran-3-ol
Synonyms
6-BROMO-2,3-DIHYDROBENZOFUNAN-3-OL;6-bromo-2,3-dihydrobenzofuran-3-ol;3-Benzofuranol, 6-bromo-2,3-dihydro-;6-bromo-2,3-dihydro-1-benzofuran-3-ol
CBNumber
CB93376725
Molecular Formula
C8H7BrO2
Formula Weight
215.04
MOL File
1392072-52-4.mol
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6-bromo-2,3-dihydrobenzofuran-3-ol Property

Boiling point:
295.0±40.0 °C(Predicted)
Density 
1.752±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
pka
13.09±0.20(Predicted)
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific
Product number
6758DT
Product name
6-Bromo-2,3-dihydrobenzofuran-3-OL
Packaging
500mg
Price
$503
Updated
2021/12/16
Crysdot
Product number
CD11266705
Product name
6-Bromo-2,3-dihydrobenzofuran-3-ol
Purity
95+%
Packaging
250mg
Price
$223
Updated
2021/12/16
Chemenu
Product number
CM122330
Product name
6-bromo-2,3-dihydrobenzofuran-3-ol
Purity
95%
Packaging
1g
Price
$421
Updated
2021/12/16
Crysdot
Product number
CD11266705
Product name
6-Bromo-2,3-dihydrobenzofuran-3-ol
Purity
95+%
Packaging
1g
Price
$446
Updated
2021/12/16
Chemenu
Product number
CM122330
Product name
6-bromo-2,3-dihydrobenzofuran-3-ol
Purity
95%
Packaging
5g
Price
$877
Updated
2021/12/16
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6-bromo-2,3-dihydrobenzofuran-3-ol Chemical Properties,Usage,Production

Synthesis

201809-69-0

1392072-52-4

1. Synthesis of (racemic)-6-bromo-2,3-dihydrobenzofuran-3-ol To a solution of 6-bromo-3-benzofuranone (10.5 g, 49.28 mmol) in methanol (100 mL) was slowly added sodium borohydride (2.37 g, 64.07 mmol) at 0 °C. Subsequently, the reaction mixture was stirred at room temperature for 2 hours. Upon completion of the reaction, the reaction was quenched with saturated ammonium chloride solution (50 mL) and extracted twice with ethyl acetate (2 x 50 mL). The organic phases were combined, dried over anhydrous sodium sulfate and concentrated under reduced pressure to give the product 6-bromo-2,3-dihydrobenzofuran-3-ol (9.75 g, 92% yield) as a colorless liquid.

References

[1] Patent: WO2012/101011, 2012, A2. Location in patent: Page/Page column 56
[2] Patent: US2013/18055, 2013, A1. Location in patent: Paragraph 0331-0332

6-bromo-2,3-dihydrobenzofuran-3-ol Preparation Products And Raw materials

Raw materials

Preparation Products

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6-bromo-2,3-dihydrobenzofuran-3-ol Suppliers

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1392072-52-4, 6-bromo-2,3-dihydrobenzofuran-3-olRelated Search:


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