ChemicalBook > CAS DataBase List > 3-IODO-1H-PYRROLO[3,2-C]PYRIDINE

3-IODO-1H-PYRROLO[3,2-C]PYRIDINE

Product Name
3-IODO-1H-PYRROLO[3,2-C]PYRIDINE
CAS No.
877060-47-4
Chemical Name
3-IODO-1H-PYRROLO[3,2-C]PYRIDINE
Synonyms
3-IODO-5-AZAINDOLE;3-Iodo-1H-pyrrolo[3,2-c]pyridin;3-IODO-1H-PYRROLO[3,2-C]PYRIDINE;1H-Pyrrolo[3,2-c]pyridine, 3-iodo-
CBNumber
CB9346963
Molecular Formula
C7H5IN2
Formula Weight
244.03
MOL File
877060-47-4.mol
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3-IODO-1H-PYRROLO[3,2-C]PYRIDINE Property

Melting point:
178-179℃
Boiling point:
380.5±22.0 °C(Predicted)
Density 
2.082
storage temp. 
2-8°C(protect from light)
pka
13.70±0.40(Predicted)
Appearance
Light yellow to yellow Solid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

AK Scientific
Product number
W9006
Product name
3-Iodo-1H-pyrrolo[3,2-c]pyridine
Packaging
5g
Price
$759
Updated
2021/12/16
Matrix Scientific
Product number
124809
Product name
3-Iodo-5-azaindole
Purity
95+%
Packaging
1g
Price
$858
Updated
2021/12/16
Ambeed
Product number
A468942
Product name
3-Iodo-5-azaindole
Purity
95%
Packaging
100mg
Price
$17
Updated
2021/12/16
Ambeed
Product number
A468942
Product name
3-Iodo-5-azaindole
Purity
95%
Packaging
250mg
Price
$26
Updated
2021/12/16
Ambeed
Product number
A468942
Product name
3-Iodo-5-azaindole
Purity
95%
Packaging
1g
Price
$58
Updated
2021/12/16
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3-IODO-1H-PYRROLO[3,2-C]PYRIDINE Chemical Properties,Usage,Production

Synthesis

271-34-1

877060-47-4

General procedure for the synthesis of 3-iodo-5-azaindole from 5-azaindole: Potassium hydroxide (KOH, 10.39 g, 185.5 mmol, 3.8 eq.) was added to a solution of 1H-pyrrolo[3,2-c]pyridine (5.76 g, 48.8 mmol, 1.0 eq.) in N,N-dimethylformamide (DMF, 30 mL). The reaction mixture was stirred at room temperature for 15 minutes. Subsequently, the reaction mixture was cooled to 0°C and a solution of iodine (I2, 12.4 g, 48.8 mmol, 1.0 eq.) in DMF (15 mL) was slowly added. After continuing to stir at room temperature for 15 min, the reaction mixture was poured into water to quench the reaction. The precipitate was separated by filtration and the solid was washed well with deionized water. Finally, the resulting yellow solid was dried under vacuum to afford 3-iodo-1H-pyrrolo[3,2-c]pyridine (9.9 g, 83% yield).

References

[1] Synthesis, 2005, # 20, p. 3581 - 3588
[2] Bioorganic and Medicinal Chemistry Letters, 2013, vol. 23, # 7, p. 2056 - 2060
[3] Patent: WO2018/11628, 2018, A1. Location in patent: Paragraph 00308
[4] Organic and Biomolecular Chemistry, 2011, vol. 9, # 14, p. 5129 - 5136

3-IODO-1H-PYRROLO[3,2-C]PYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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3-IODO-1H-PYRROLO[3,2-C]PYRIDINE Suppliers

JinYan Chemicals(ShangHai) Co.,Ltd.
Tel
13817811078
Fax
86-021-50426522,50426273
Email
sales@jingyan-chemical.com
Country
China
ProdList
9976
Advantage
60
Pure Chemistry Scientific Inc.
Tel
001-857-928-2050 or 1-888-588-9418
Fax
001-617-206-9595
Email
sales@chemreagents.com
Country
United States
ProdList
10186
Advantage
62
Shandong Xiya Chemical Co., Ltd
Tel
4009903999 13355009207
Fax
0539-6365991
Email
3007715519@qq.com
Country
China
ProdList
18729
Advantage
57
Wuhan ariel chemical Co., LTD.
Tel
18986259541
Fax
027-87840182
Email
sales@3stc.com
Country
China
ProdList
3764
Advantage
58
Shanghai Xiannuo Biotechnology Co., Ltd.
Tel
021-50718719 13918719472
Fax
021-50718719
Country
China
ProdList
979
Advantage
58
Shijiazhuang suchen Chemical Technology Co. LTD
Tel
186-33933494 18032288352
Fax
0311-85310887
Email
1130239@qq.com
Country
China
ProdList
202
Advantage
60
Runpharm Technology Limited
Tel
18171398856 2968382473
Fax
0086-21-50758330
Email
service@runpharm.com
Country
China
ProdList
716
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Wuhan Kaymke Chemical Co., Ltd.,
Tel
027-027-87342388 18086026008
Fax
027-87342388
Email
sales@kaymke.com
Country
China
ProdList
3732
Advantage
55
Shanghai Yolne Chemical Co., Ltd.
Tel
021-62960152
Fax
021-52212593
Email
934678158@qq.com
Country
China
ProdList
9899
Advantage
55
Chengdu AstaTech Trading Co., Ltd./AstaTech (Chengdu) Pharma. Co., Ltd.
Tel
+86-28-85122536 85324413
Fax
+86-28-85326443
Email
market@astatech.cn
Country
China
ProdList
8026
Advantage
55
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View Lastest Price from 3-IODO-1H-PYRROLO[3,2-C]PYRIDINE manufacturers

Career Henan Chemical Co
Product
3-IODO-1H-PYRROLO[3,2-C]PYRIDINE 877060-47-4
Price
US $1.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
1kg; 2kg;10kg; 100kg
Release date
2019-08-30