ChemicalBook > CAS DataBase List > 5-(3-CHLORO-PHENYL)-[1,3,4]THIADIAZOL-2-YLAMINE

5-(3-CHLORO-PHENYL)-[1,3,4]THIADIAZOL-2-YLAMINE

Product Name
5-(3-CHLORO-PHENYL)-[1,3,4]THIADIAZOL-2-YLAMINE
CAS No.
70057-67-9
Chemical Name
5-(3-CHLORO-PHENYL)-[1,3,4]THIADIAZOL-2-YLAMINE
Synonyms
5-(3-CHLOROPHENYL)-1,3,4-THIADIAZOL-2-AMINE;2-Amino-5-(3-chlorophenyl)-1,3,4-thiadiazole;1,3,4-Thiadiazol-2-amine, 5-(3-chlorophenyl)-;5-(3-CHLORO-PHENYL)-[1,3,4]THIADIAZOL-2-YLAMINE
CBNumber
CB9424119
Molecular Formula
C8H6ClN3S
Formula Weight
211.67
MOL File
Mol file
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5-(3-CHLORO-PHENYL)-[1,3,4]THIADIAZOL-2-YLAMINE Property

storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
C350820
Product name
5-(3-Chlorophenyl)-1,3,4-thiadiazol-2-amine
Packaging
10mg
Price
$45
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0035245
Product name
5-(3-CHLOROPHENYL)-1,3,4-THIADIAZOL-2-AMINE
Purity
95.00%
Packaging
250MG
Price
$307.65
Updated
2021/12/16
AK Scientific
Product number
Y2773
Product name
5-(3-Chlorophenyl)-1,3,4-thiadiazol-2-amine
Packaging
1g
Price
$324
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0035245
Product name
5-(3-CHLOROPHENYL)-1,3,4-THIADIAZOL-2-AMINE
Purity
95.00%
Packaging
1G
Price
$852.55
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0035245
Product name
5-(3-CHLOROPHENYL)-1,3,4-THIADIAZOL-2-AMINE
Purity
95.00%
Packaging
2.5G
Price
$1227.82
Updated
2021/12/16
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5-(3-CHLORO-PHENYL)-[1,3,4]THIADIAZOL-2-YLAMINE Chemical Properties,Usage,Production

Synthesis

79-19-6

535-80-8

70057-67-9

5.1.1 Synthesis of 5-(3-chlorophenyl)-1,3,4-thiadiazol-2-amine (67): 3-chlorobenzoic acid (5.18 g, 25 mmol) and N-amino thiourea (2.28 g, 25 mmol) were dissolved in POCl3 (7 ml), and the reaction was stirred vigorously for 0.5 hr at 75 °C. After completion of the reaction, H2O (30 ml) was added and the reaction mixture was heated to reflux for 4 hours. Subsequently, the reaction solution was adjusted with 50% NaOH solution to pH 8. The reaction mixture was filtered and the filter cake was recrystallized with ethanol to give the target product 67 as yellow crystals. Yield: 75%; Melting point: 212-214 °C (EtOH). eSI-MS m/z: 212.1 [M + H]+; 1H NMR (CDCl3) δ 7.49-7.50 (m, 2H), 7.54 (s, 2H), 7.70-7.71 (m, 1H), 7.80 (s, 1H).

References

[1] Journal of Chemical Research, 2011, vol. 35, # 12, p. 703 - 706
[2] Bioorganic and Medicinal Chemistry, 2014, vol. 22, # 21, p. 5766 - 5775
[3] Journal of Chemical Research, 2012, vol. 36, # 4, p. 218 - 221
[4] Pharmazie, 2018, vol. 73, # 3, p. 123 - 127
[5] Bioorganic Chemistry, 2018, vol. 81, p. 88 - 92

5-(3-CHLORO-PHENYL)-[1,3,4]THIADIAZOL-2-YLAMINE Preparation Products And Raw materials

Raw materials

Preparation Products

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5-(3-CHLORO-PHENYL)-[1,3,4]THIADIAZOL-2-YLAMINE Suppliers

China 20 Hungary 1 India 2 Russia 1 Ukraine 1 United Kingdom 3 United States 2 Global 30
Changzhou Hopschain Chemical Co.,Ltd.
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Amadis Chemical Company Limited
Tel
571-89925085
Fax
0086-571-89925065
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Aikon International Limited
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Suzhou Victorypharm Co.,Ltd.
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Changzhou Yinghao Technology Development Co., Ltd
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Zhengzhou Alpha Chemical Co. LTD
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Hefei Mokai Pharmaceutical Technology Co., Ltd
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Bide Pharmatech Ltd.
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Bide Pharmatech Ltd.
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Suzhou Victorypharm Co.,Ltd.
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70057-67-9, 5-(3-CHLORO-PHENYL)-[1,3,4]THIADIAZOL-2-YLAMINERelated Search:


  • 5-(3-CHLOROPHENYL)-1,3,4-THIADIAZOL-2-AMINE
  • 5-(3-CHLORO-PHENYL)-[1,3,4]THIADIAZOL-2-YLAMINE
  • 1,3,4-Thiadiazol-2-amine, 5-(3-chlorophenyl)-
  • 2-Amino-5-(3-chlorophenyl)-1,3,4-thiadiazole
  • 70057-67-9