2-AMINO-5-BROMO-3-METHYLBENZOIC ACID
Uses- Product Name
- 2-AMINO-5-BROMO-3-METHYLBENZOIC ACID
- CAS No.
- 206548-13-2
- Chemical Name
- 2-AMINO-5-BROMO-3-METHYLBENZOIC ACID
- Synonyms
- BUTTPARK 76\07-03;2-Amino-5-bromo-3-methylbenzoicaci;2-AMINO-5-BROMO-3-METHYLBENZOIC ACID;Benzoic acid, 2-amino-5-bromo-3-methyl-
- CBNumber
- CB9444463
- Molecular Formula
- C8H8BrNO2
- Formula Weight
- 230.06
- MOL File
- Mol file
2-AMINO-5-BROMO-3-METHYLBENZOIC ACID Property
- Melting point:
- 236-238°C
- Boiling point:
- 347.9±42.0 °C(Predicted)
- Density
- 1.682
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 4.62±0.10(Predicted)
- Appearance
- White to off-white Solid
Safety
- HS Code
- 2922498590
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H226Flammable liquid and vapour
H315Causes skin irritation
H317May cause an allergic skin reaction
H319Causes serious eye irritation
H400Very toxic to aquatic life
- Precautionary statements
-
P210Keep away from heat/sparks/open flames/hot surfaces. — No smoking.
P233Keep container tightly closed.
P240Ground/bond container and receiving equipment.
P241Use explosion-proof electrical/ventilating/lighting/…/equipment.
P242Use only non-sparking tools.
P243Take precautionary measures against static discharge.
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P272Contaminated work clothing should not be allowed out of the workplace.
P273Avoid release to the environment.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P303+P361+P353IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P333+P313IF SKIN irritation or rash occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
P370+P378In case of fire: Use … for extinction.
P391Collect spillage. Hazardous to the aquatic environment
P403+P235Store in a well-ventilated place. Keep cool.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- A576918
- Product name
- 2-Amino-5-bromo-3-methylbenzoicAcid
- Packaging
- 50mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- HCH0328089
- Product name
- 2-AMINO-5-BROMO-3-METHYLBENZOIC ACID
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $498.44
- Updated
- 2021/12/16
- Product number
- J97275
- Product name
- 2-Amino-5-bromo-3-methylbenzoicacid
- Packaging
- 25g
- Price
- $510
- Updated
- 2021/12/16
- Product number
- FA11525
- Product name
- 2-Amino-5-bromo-3-methylbenzoic acid
- Packaging
- 10g
- Price
- $680
- Updated
- 2021/12/16
- Product number
- FA11525
- Product name
- 2-Amino-5-bromo-3-methylbenzoic acid
- Packaging
- 25g
- Price
- $1360
- Updated
- 2021/12/16
2-AMINO-5-BROMO-3-METHYLBENZOIC ACID Chemical Properties,Usage,Production
Uses
2-AMINO-5-BROMO-3-METHYLBENZOIC ACID is a useful research chemical.
Synthesis
4389-45-1
206548-13-2
Step A: 2-Amino-3-methylbenzoic acid (10.0 g, 66 mmol) was dissolved in DMSO, followed by the addition of 48% aqueous hydrogen bromide solution (18.0 mL). The reaction mixture was stirred at room temperature overnight, and upon completion of the reaction, the reaction was quenched with saturated sodium bicarbonate solution. The resulting mixture was continued to be stirred overnight and the precipitate was subsequently collected by filtration and dried under vacuum to afford 2-amino-5-bromo-3-methylbenzoic acid (13.0 g, 85% yield) as a pink solid. The product was characterized by 1H NMR (500 MHz, DMSO): δ 7.69 (d, J = 1.0 Hz, 1H), 7.33 (d, J = 1.0 Hz, 1H), 2.10 (s, 3H); mass spectrum (ESI+) m/z 231 ([M + H]+).
References
[1] Patent: EP2842946, 2015, A1. Location in patent: Paragraph 0309; 0728; 0729
[2] Journal of Agricultural and Food Chemistry, 2012, vol. 60, # 44, p. 10942 - 10951
[3] Journal of Organic Chemistry, 2006, vol. 71, # 16, p. 5921 - 5929
[4] Patent: WO2011/8572, 2011, A2. Location in patent: Page/Page column 70
[5] Patent: WO2008/65508, 2008, A1. Location in patent: Page/Page column 29-30
2-AMINO-5-BROMO-3-METHYLBENZOIC ACID Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-AMINO-5-BROMO-3-METHYLBENZOIC ACID manufacturers
- Product
- 2-AMINO-5-BROMO-3-METHYLBENZOIC ACID 206548-13-2
- Price
- US $1.00/ASSAYS
- Min. Order
- 1ASSAYS
- Purity
- 85.0-99.8%
- Supply Ability
- 20tons
- Release date
- 2020-01-08