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Monomethyl adipate

Product Name
Monomethyl adipate
CAS No.
627-91-8
Chemical Name
Monomethyl adipate
Synonyms
6-Methoxy-6-oxohexanoic acid;Adipic acid monometh;ADIPIC ACID MONOMETHYL ESTER;NSC55113;NSC 55113;NSC-55113;METHYL ADIPATE;Methyladipinate;Methyl hemiadipate;MONO-METHYL ADIPATE
CBNumber
CB9683693
Molecular Formula
C7H12O4
Formula Weight
160.17
MOL File
627-91-8.mol
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Monomethyl adipate Property

Melting point:
7-9 °C (lit.)
Boiling point:
162 °C/10 mmHg (lit.)
Density 
1.081 g/mL at 25 °C (lit.)
vapor pressure 
1.48Pa at 25℃
refractive index 
n20/D 1.441(lit.)
Flash point:
>230 °F
storage temp. 
Sealed in dry,Room Temperature
solubility 
Chloroform (Sparingly), Methanol (Slightly)
form 
Liquid
pka
4.69±0.10(Predicted)
color 
Clear colorless
Water Solubility 
Not miscible or difficult to mix with water.
BRN 
1766411
LogP
0.500 (est)
CAS DataBase Reference
627-91-8(CAS DataBase Reference)
NIST Chemistry Reference
Hexanedioic acid, monomethyl ester(627-91-8)
EPA Substance Registry System
Monomethyl adipate (627-91-8)
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
24/25-36-26
WGK Germany 
3
TSCA 
Yes
HS Code 
29171290
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
A26403
Product name
mono-Methyl adipate
Purity
99%
Packaging
5g
Price
$35.34
Updated
2024/03/01
Sigma-Aldrich
Product number
A26403
Product name
mono-Methyl adipate
Purity
99%
Packaging
25g
Price
$101
Updated
2024/03/01
TCI Chemical
Product number
A1738
Product name
Monomethyl Adipate
Purity
>97.0%(GC)(T)
Packaging
25g
Price
$66
Updated
2024/03/01
TCI Chemical
Product number
A1738
Product name
Monomethyl Adipate
Purity
>97.0%(GC)(T)
Packaging
100g
Price
$201
Updated
2024/03/01
Alfa Aesar
Product number
L09061
Product name
Methyl hydrogen adipate, 99%
Packaging
25g
Price
$87.9
Updated
2021/12/16
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Monomethyl adipate Chemical Properties,Usage,Production

Chemical Properties

clear colorless liquid

Uses

Methyl hydrogen adipate is a useful synthetic intermediate. It can be used to prepare 1,3,4-thiadiazole hydroxamic acid derivatives as novel histone deacetylase inhibitors which show potential antitumor activities. It can be also used to synthesize mannose-linked biphenylylacetic acid derivatives as novel inhibitors of selectin-mediated cell adhesion.

Definition

ChEBI: Monomethyl adipate is a dicarboxylic acid monoester that is the monomethyl ester of adipic acid. It has a role as a metabolite and a plasticiser.

Synthesis

According to the general procedure described above, a has been synthesized from adipic acid (730mg, 5 mmol) and methanol (10 ml). Yield: 80%.
The synthetic method of Monomethyl adipate mainly contains following three kinds:
The one, under alkaline condition or issue the first portion hydrolysis reaction in the catalysis of bioactive enzyme (pork liver lipase etc.) and obtain Monomethyl adipate (such as document Blaise; Koehler; Bulletin de la Societe Chimique deFrance; Vol. (4) 7; (1910); P.219).
The 2nd, by hexanodioic acid or adipic anhydride and ethanol, as catalyzer, the control reaction conditions carries out esterification and obtains Monomethyl adipate (such as document Chem.Zentralbl. with acid; Vol.97; (1926; P.126));
The 3rd, by the people such as Swann nineteen forty-three with hexanodioic acid, diethylene adipate and ethanol with the condition of acid as catalyst under control reaction conditions obtain monomethyl adipate(document such as Swann; Oehler; Buswell; Org.synth.Coll.Vol.11; (1943); P.227).
Synthetic method of monomethyl adipate
http://www.orgsyn.org/demo.aspx?prep=CV2P0264

Monomethyl adipate Preparation Products And Raw materials

Raw materials

Preparation Products

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Monomethyl adipate Suppliers

TOKYO CHEMICAL INDUSTRY CO., LTD.
Tel
03-36680489
Fax
03-3668-0520
Email
Sales-JP@TCIchemicals.com
Country
Japan
ProdList
28387
Advantage
80
Hattori Corporation
Tel
--
Fax
--
Email
info@hattoricorp.com
Country
Japan
ProdList
1254
Advantage
58
K. Sakai & Co., Ltd.
Tel
--
Fax
--
Email
em@ksakai.co.jp
Country
Japan
ProdList
957
Advantage
58
Nacalai Tesque, Inc.
Tel
--
Fax
--
Email
info-tech@nacalai.co.jp
Country
Japan
ProdList
6046
Advantage
75
Kanto Chemical Co., Inc.
Tel
--
Fax
--
Email
reag-info@gms.kanto.co.jp
Country
Japan
ProdList
6756
Advantage
74
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View Lastest Price from Monomethyl adipate manufacturers

Hebei Zhuanglai Chemical Trading Co.,Ltd
Product
Monomethyl adipate 627-91-8
Price
US $50.00/kg
Min. Order
1kg
Purity
99
Supply Ability
5000
Release date
2024-04-30
Hebei Chuanghai Biotechnology Co,.LTD
Product
Monomethyl adipate 627-91-8
Price
US $100.00-50.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
10000kg
Release date
2024-08-20
Hebei Weibang Biotechnology Co., Ltd
Product
Monomethyl adipate 627-91-8
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
10 mt
Release date
2022-10-11

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