ChemicalBook > CAS DataBase List > N-(4-BROMOPHENYL)MORPHOLINE

N-(4-BROMOPHENYL)MORPHOLINE

Product Name
N-(4-BROMOPHENYL)MORPHOLINE
CAS No.
30483-75-1
Chemical Name
N-(4-BROMOPHENYL)MORPHOLINE
Synonyms
N-(4-BROMOPHENYL)MORPHOLINE;1-Bromo-4-morpholinobenzene;4-(4'-BROMOPHENYL)MORPHOLINE;Morpholine,4-(4-bromophenyl)-;4-(4-Bromophenyl)morpholine 97%
CBNumber
CB9697164
Molecular Formula
C10H12BrNO
Formula Weight
242.11
MOL File
30483-75-1.mol
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N-(4-BROMOPHENYL)MORPHOLINE Property

Melting point:
114-118 °C (lit.)
Boiling point:
341.2±37.0 °C(Predicted)
Density 
1.433±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
form 
powder to crystal
pka
4.33±0.40(Predicted)
color 
White to Light yellow to Light orange
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-36
WGK Germany 
3
HS Code 
2934999090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
591777
Product name
4-(4-Bromophenyl)morpholine
Purity
97%
Packaging
5g
Price
$58.8
Updated
2024/03/01
Sigma-Aldrich
Product number
591777
Product name
4-(4-Bromophenyl)morpholine
Purity
97%
Packaging
25g
Price
$259
Updated
2024/03/01
TCI Chemical
Product number
B4890
Product name
4-(4-Bromophenyl)morpholine
Purity
>98.0%(GC)(T)
Packaging
5g
Price
$129
Updated
2024/03/01
TCI Chemical
Product number
B4890
Product name
4-(4-Bromophenyl)morpholine
Purity
>98.0%(GC)(T)
Packaging
25g
Price
$381
Updated
2023/01/07
TRC
Product number
B678033
Product name
4-(4-Bromophenyl)morpholine
Packaging
500mg
Price
$75
Updated
2021/12/16
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N-(4-BROMOPHENYL)MORPHOLINE Chemical Properties,Usage,Production

Uses

N-(4-BROMOPHENYL)MORPHOLINE is used as organic synthesis intermediate and pharmaceutical intermediate, mainly used in laboratory research and development process and chemical production process.

Synthesis


In an open flask, 10 mL of 1.5 M NaBr in pH 6.2 phosphate buffer (0.23 M in PO4) or pH 4.2 phosphate buffer (5% NaH2PO4) was added to a solution of 1 mmol of substrate dissolved in 9.75 mL of distilled 1,4- dioxane. To this mixture was added a freshly made solution of diphenyl ditelluride (1e, 0.25 mL of a 10 mM stock in 1,4-dioxane, 2.5 μmol, 0.25 mol % relative to substrate) followed by the addition of 8.8 M H2O2 according to Table 3. The reaction mixture was stirred at room temperature for the appropriate amount of time and was then diluted with 10 mL of water. The resulting solution was extracted with EtOAc (3 × 10 mL), and the combined organic extracts were washed with 0.5 M NaHSO3 (5 mL) and brine (10 mL), dried over MgSO4, and concentrated. Yields reported below are the mean of duplicate runs. N-(4-Bromophenyl)morpholine (21):28 product isolated as a tan solid (224 ± 1 mg, 93% yield). Mp 111-113 °C (lit.28 mp 111-112 °C).

N-(4-BROMOPHENYL)MORPHOLINE Preparation Products And Raw materials

Raw materials

Preparation Products

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N-(4-BROMOPHENYL)MORPHOLINE Suppliers

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30483-75-1, N-(4-BROMOPHENYL)MORPHOLINERelated Search:

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  • N-(4-BROMOPHENYL)MORPHOLINE
  • 4-(4'-BROMOPHENYL)MORPHOLINE
  • 1-Bromo-4-morpholinobenzene
  • 4-(4-Bromophenyl)morpholine 97%
  • Morpholine,4-(4-bromophenyl)-
  • 30483-75-1
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