ChemicalBook > CAS DataBase List > 2-Iodo-1-methyl-1H-imidazole

2-Iodo-1-methyl-1H-imidazole

Product Name
2-Iodo-1-methyl-1H-imidazole
CAS No.
37067-95-1
Chemical Name
2-Iodo-1-methyl-1H-imidazole
Synonyms
2-IODO-1-METHYLIMIDAZOLE;2-IODO-1-METHYL-1H-IMIDAZOLE;1H-Imidazole, 2-iodo-1-methyl-;2-Iodo-1-methyl-1H-imidazole
CBNumber
CB9723285
Molecular Formula
C4H5IN2
Formula Weight
208
MOL File
37067-95-1.mol
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2-Iodo-1-methyl-1H-imidazole Property

Melting point:
87 °C
Boiling point:
120-122°C 45mm
Density 
2.07±0.1 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
form 
solid
pka
4.17±0.25(Predicted)
Appearance
Off-white to light brown Solid
Sensitive 
Light Sensitive
InChI
InChI=1S/C4H5IN2/c1-7-3-2-6-4(7)5/h2-3H,1H3
InChIKey
BKRACZNEJSCZML-UHFFFAOYSA-N
SMILES
C1(I)N(C)C=CN=1
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Safety

Hazard Codes 
Xi,Xn
Risk Statements 
36/37/38-22-41-37/38
Safety Statements 
26-36/37/39-22-39
WGK Germany 
3
Hazard Note 
Irritant
HS Code 
2933299090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Danger
Hazard statements

H315Causes skin irritation

H318Causes serious eye damage

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
CDS005078
Product name
2-Iodo-1-methyl-1H-imidazole
Purity
Aldrich
Packaging
100mg
Price
$73.1
Updated
2025/07/31
Sigma-Aldrich
Product number
ANV00120
Product name
2-Iodo-1-methyl-1H-imidazole
Purity
AldrichCPR
Packaging
1G
Price
$286
Updated
2025/07/31
AK Scientific
Product number
Y8898
Product name
2-Iodo-1-methyl-1H-imidazole
Packaging
250mg
Price
$39
Updated
2021/12/16
SynQuest Laboratories
Product number
3H32-H-X6
Product name
2-Iodo-1-methyl-1H-imidazole
Packaging
250mg
Price
$96
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0020054
Product name
2-IODO-1-METHYL-1H-IMIDAZOLE
Purity
95.00%
Packaging
250MG
Price
$664.82
Updated
2021/12/16
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2-Iodo-1-methyl-1H-imidazole Chemical Properties,Usage,Production

Synthesis

616-47-7

37067-95-1

GENERAL METHOD: To a mixture containing 2-phenylimidazo[1,2-a]pyridine (1a, 39 mg, 0.2 mmol), molecular iodine (I2, 50 mg, 0.2 mmol), and 4-(3-methylimidazolyl)butane-1-sulfonate (I, 9 mg, 0.04 mmol), water (2 mL) was added. The mixture was transferred to a sealed tube and stirred at room temperature for 2 hours. After completion of the reaction (monitored by TLC), the mixture was extracted with ethyl acetate (20 mL). The organic phase was dried with anhydrous sodium sulfate (Na2SO4) and concentrated under reduced pressure to give the crude product. The crude product was purified by column chromatography (silica gel, 60-120 mesh, petroleum ether/ethyl acetate, 9:1) to give 2-iodo-1-methyl-1H-imidazole (2a) as a white solid. Yield: 58 mg (91%); melting point: 132-134 °C.

References

[1] Organic Letters, 2014, vol. 16, # 12, p. 3244 - 3247
[2] European Journal of Inorganic Chemistry, 2017, vol. 2017, # 20, p. 2774 - 2781
[3] Organic Letters, 2003, vol. 5, # 18, p. 3209 - 3212
[4] Journal of Organometallic Chemistry, 2007, vol. 692, # 1-3, p. 635 - 644
[5] Synthesis (Germany), 2016, vol. 48, # 22, p. 4009 - 4015

2-Iodo-1-methyl-1H-imidazole Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-Iodo-1-methyl-1H-imidazole manufacturers

Career Henan Chemical Co
Product
2-Iodo-1-methyl-1H-imidazole 37067-95-1
Price
US $1.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
1kg,5kg,100kg
Release date
2019-07-04

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