ChemicalBook > CAS DataBase List > 4-(3-BROMO-PHENYL)-1H-IMIDAZOLE

4-(3-BROMO-PHENYL)-1H-IMIDAZOLE

Product Name
4-(3-BROMO-PHENYL)-1H-IMIDAZOLE
CAS No.
53848-00-3
Chemical Name
4-(3-BROMO-PHENYL)-1H-IMIDAZOLE
Synonyms
4-(3-BROMO-PHENYL)-1H-IMIDAZOLE;1H-Imidazole, 5-(3-bromophenyl)-
CBNumber
CB9848513
Molecular Formula
C9H7BrN2
Formula Weight
223.07
MOL File
53848-00-3.mol
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4-(3-BROMO-PHENYL)-1H-IMIDAZOLE Property

Boiling point:
412.8±20.0 °C(Predicted)
Density 
1.565±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
pka
13.21±0.10(Predicted)
Appearance
Off-white to light yellow Solid
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P312Call a POISON CENTER or doctor/physician if you feel unwell.

P321Specific treatment (see … on this label).

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

P362Take off contaminated clothing and wash before reuse.

P403+P233Store in a well-ventilated place. Keep container tightly closed.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

American Custom Chemicals Corporation
Product number
HCH0366489
Product name
5-(3-BROMOPHENYL)-1H-IMIDAZOLE
Purity
95.00%
Packaging
5MG
Price
$496.69
Updated
2021/12/16
Ambeed
Product number
A109053
Product name
5-(3-Bromophenyl)-1H-imidazole
Purity
95+%
Packaging
100mg
Price
$82
Updated
2021/12/16
Ambeed
Product number
A109053
Product name
5-(3-Bromophenyl)-1H-imidazole
Purity
95+%
Packaging
250mg
Price
$82
Updated
2021/12/16
Ambeed
Product number
A109053
Product name
5-(3-Bromophenyl)-1H-imidazole
Purity
95+%
Packaging
1g
Price
$127
Updated
2021/12/16
Crysdot
Product number
CD11108585
Product name
5-(3-Bromophenyl)-1H-imidazole
Purity
95+%
Packaging
1g
Price
$342
Updated
2021/12/16
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4-(3-BROMO-PHENYL)-1H-IMIDAZOLE Chemical Properties,Usage,Production

Synthesis

618-44-0

77287-34-4

53848-00-3

General method: α-Bromophenyl ketone derivative (1.34 mmol) was dissolved in formamide (10 mL) and the reaction was heated at 170-180°C for 5-10 hours. After completion of the reaction, the reaction solution was cooled to room temperature and diluted with saturated NaHCO3 solution (20 mL). Subsequently, the aqueous phase was extracted with ethyl acetate (3 x 50 mL). The organic layers were combined, washed sequentially with water and saturated brine and dried over anhydrous Na2SO4. The organic phase was concentrated under reduced pressure to obtain the crude product. Finally, the crude product was purified by silica gel fast column chromatography to obtain the target compound 5-(3-bromophenyl)-1H-imidazole.

References

[1] Patent: US9174942, 2015, B2. Location in patent: Page/Page column 204

4-(3-BROMO-PHENYL)-1H-IMIDAZOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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4-(3-BROMO-PHENYL)-1H-IMIDAZOLE Suppliers

SynAsst Chemical.
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