ChemicalBook > CAS DataBase List > 2,2,2-TRIFLUORO-1-(4-IODO-PHENYL)-ETHANONE

2,2,2-TRIFLUORO-1-(4-IODO-PHENYL)-ETHANONE

Product Name: 2,2,2-TRIFLUORO-1-(4-IODO-PHENYL)-ETHANONE
CAS No.: 23516-84-9
Chemical Name: 2,2,2-TRIFLUORO-1-(4-IODO-PHENYL)-ETHANONE
Synonyms: 4-Iodotrifluoroacetophenone;2,2,2-TRIFLUORO-1-(4-IODO-PHENYL)-ETHANONE;Ethanone, 2,2,2-trifluoro-1-(4-iodophenyl)-;2,2,2-Trifluoro-1-(4-iodophenyl)ethan-1-one
CBNumber: CB9849828
Molecular Formula: C8H4F3IO
Formula Weight: 300.02
MOL File: 23516-84-9.mol

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2,2,2-TRIFLUORO-1-(4-IODO-PHENYL)-ETHANONE Property

Boiling point:: 260.3±40.0 °C(Predicted)
Density: 1.881±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
Appearance: Colorless to off-white Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

Matrix Scientific

Product number: 094620
Product name: 2,2,2-Trifluoro-1-(4-iodophenyl)ethanone
Purity: 95+%
Packaging: 250mg
Price: $364
Updated: 2021/12/16

AK Scientific

Product number: 1592AB
Product name: 2,2,2-Trifluoro-1-(4-iodophenyl)ethanone
Packaging: 1g
Price: $450
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2617-K-02
Product name: 2,2,2-Trifluoro-1-(4-iodophenyl)ethan-1-one
Purity: 97%
Packaging: 250mg
Price: $491
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0103569
Product name: 2,2,2-TRIFLUORO-1-(4-IODO-PHENYL)-ETHANONE
Purity: 95.00%
Packaging: 5MG
Price: $495.73
Updated: 2021/12/16

Matrix Scientific

Product number: 094620
Product name: 2,2,2-Trifluoro-1-(4-iodophenyl)ethanone
Purity: 95+%
Packaging: 1g
Price: $807
Updated: 2021/12/16

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2,2,2-TRIFLUORO-1-(4-IODO-PHENYL)-ETHANONE Chemical Properties,Usage,Production

Synthesis

619-44-3

81290-20-2

1214788-34-7

23516-84-9

Preparation of the intermediate tert-butyl, 1,1,3,3,3-hexafluoro-2-(4-iodobenzyl)DroDan-2-yloxy)dimethylsilane (1V-1): 4-Iodobenzoic acid methyl ester (5 g, 19.08 mmol) was dissolved in tetrahydrofuran (80 mL) and cooled to 0 °C. (Trifluoromethyl)trimethylsilane (5.43 g, 38.2 mmol) and cesium fluoride (145 mg, 0.954 mmol) were added sequentially. After the addition was completed, the reaction system was slowly warmed to room temperature and stirred continuously for 3 hours. Subsequently, (trifluoromethyl)trimethylsilane (2.715 g, 19.08 mmol) was added additionally and the reaction continued to be stirred at room temperature for 4 hours. After completion of the reaction, the reaction was quenched by the addition of 4M aqueous hydrochloric acid (20 mL) and stirred for 5 hours. The reaction mixture was diluted with ethyl acetate (500 mL), washed sequentially with water (2 x 250 mL), the organic phase was dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure. The crude product was purified by silica gel column chromatography using a 0% to 10% ethyl acetate/heptane gradient elution to isolate 2,2,2-trifluoro-1-(4-iodophenyl)ethanone (1.8 g, 31% yield), GCMS: m/z = 300, retention time 1.47 min; and 1,1,1,3,3,3-hexafluoro-2-(4-iodophenyl)propan-2-ol (1.6 g, 22% yield), GCMS: m/z = 370, retention time 160 min.

References

[1] Patent: WO2010/86820, 2010, A1. Location in patent: Page/Page column 46
[2] Patent: US2010/197591, 2010, A1. Location in patent: Page/Page column 21

2,2,2-TRIFLUORO-1-(4-IODO-PHENYL)-ETHANONE Preparation Products And Raw materials

Raw materials

Preparation Products

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23516-84-9, 2,2,2-TRIFLUORO-1-(4-IODO-PHENYL)-ETHANONERelated Search:

2,2,2-TRIFLUORO-1-(2-IODO-PHENYL)-ETHANONE 2,2,2-TRIFLUORO-1-(4-IODO-PHENYL)-ETHANONE OXIME 2,2,2-TRIFLUORO-1-(3-IODO-PHENYL)-ETHANONE 2,2,2-TRIFLUORO-1-(4-IODO-PHENYL)-ETHANONE

2,2,2-Trifluoro-1-(4-iodophenyl)ethan-1-one

4-Iodotrifluoroacetophenone

2,2,2-TRIFLUORO-1-(4-IODO-PHENYL)-ETHANONE

Ethanone, 2,2,2-trifluoro-1-(4-iodophenyl)-

23516-84-9

C8H4F3IO