9-(2-nitrovinyl)anthracene

Product Name: 9-(2-nitrovinyl)anthracene
CAS No.: 58349-77-2
Chemical Name: 9-(2-nitrovinyl)anthracene
Synonyms: Einecs 261-220-2;9-(2-nitrovinyl)anthracene;9-(2-Nitroethenyl)anthracene;Anthracene,9-(2-nitroethenyl)-;(E)-9-(2-Nitrovinyl)anthracene
CBNumber: CB9883909
Molecular Formula: C16H11NO2
Formula Weight: 249.26
MOL File: 58349-77-2.mol

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9-(2-nitrovinyl)anthracene Property

storage temp.: 2-8°C

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

H412Harmful to aquatic life with long lasting effects

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P273Avoid release to the environment.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Ambeed

Product number: A245447
Product name: 9-(2-Nitrovinyl)anthracene
Purity: 97%
Packaging: 100mg
Price: $59
Updated: 2021/12/16

Ambeed

Product number: A245447
Product name: 9-(2-Nitrovinyl)anthracene
Purity: 97%
Packaging: 250mg
Price: $87
Updated: 2021/12/16

Ambeed

Product number: A245447
Product name: 9-(2-Nitrovinyl)anthracene
Purity: 97%
Packaging: 1g
Price: $235
Updated: 2021/12/16

Crysdot

Product number: CD12058635
Product name: 9-(2-Nitrovinyl)anthracene
Purity: 97%
Packaging: 1g
Price: $270
Updated: 2021/12/16

Abosyn

Product number: 61-10481
Product name: 9-(2-Nitrovinyl)anthracene
Purity: 95-98%
Packaging: 1g
Price: $315
Updated: 2021/12/16

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9-(2-nitrovinyl)anthracene Chemical Properties,Usage,Production

Synthesis

75-52-5

642-31-9

58349-77-2

GENERAL METHOD: 9-Anthracenecarboxaldehyde (1; 2.06 g, 10 mmol) was dissolved in anhydrous dichloromethane (20 mL). To this solution nitromethane (559 μL, 10 mmol) and piperidine (202 μL, 2 mmol) were added sequentially. The reaction mixture was heated to reflux and maintained for 8 hours. After completion of the reaction, it was cooled to room temperature and a red solid precipitated. The solid product was collected by filtration and washed with hexane (20 mL) to afford the target compound 9-(2-nitrovinyl)anthracene (1.70 g, 68% yield) as a red solid. Compound Registry Number: 55446-60-1; Thin Layer Chromatography Rf value = 0.56 (Expanding Agent Ratio: Hexane:Ethyl Acetate = 80:20); 1H NMR (CDCl3, 300 MHz) δ = 7.49-7.65 (m, 5H, aromatic hydrogens and -CH=CHNO2), 8.07 (d, J=7.9 Hz, 2H, aromatic hydrogens), 8.20 (d, J=8.8 Hz, 2H, aromatic hydrogen), 8.56 (s, 1H, H-10), 9.03 (d, J=13.8 Hz, 1H, -CH=CHNO2). Ref: Becker, H.D.; Soerensen, H.; Sandros, K. J. Org. Chem. 1986, 51, 3223-3226.

References

[1] Tetrahedron Letters, 2013, vol. 54, # 32, p. 4306 - 4308
[2] Doklady Chemistry, 1975, vol. 225, p. 681 - 684
[3] Dokl. Akad. Nauk SSSR Ser. Khim., 1975, vol. 225, # 6, p. 1323 - 1326
[4] Inorganica Chimica Acta, 2015, vol. 426, p. 119 - 125
[5] Synthetic Communications, 2017, vol. 47, # 6, p. 551 - 556

9-(2-nitrovinyl)anthracene Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 9-(2-nitrovinyl)anthracene manufacturers

Career Henan Chemical Co

Product: 9-(2-nitrovinyl)anthracene 58349-77-2
Price: US $1.00/g
Min. Order: 1g
Purity: 99.0%
Supply Ability: 100kg
Release date: 2020-01-09

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