1-(2-Hydroxy-4,6-dimethoxyphenyl)-2-(4-methoxyphenyl)ethanone CAS#: 39604-68-7

1-(2-Hydroxy-4,6-dimethoxyphenyl)-2-(4-methoxyphenyl)ethanone Basic information

Product Name:

1-(2-Hydroxy-4,6-dimethoxyphenyl)-2-(4-methoxyphenyl)ethanone

Synonyms:

2'-Hydroxy-4',6'-dimethoxy-2-(4-methoxyphenyl)acetophenone
JR-6463, 1-(2-Hydroxy-4,6-dimethoxyphenyl)-2-(4-methoxyphenyl)ethanone, 97%
Ethanone, 1-(2-hydroxy-4,6-dimethoxyphenyl)-2-(4-methoxyphenyl)-
2-Hydroxy-4,6-dimethoxyphenyl 4-Methoxybenzyl Ketone
1-(2-Hydroxy-4,6-dimethoxyphenyl)-2-(4-methoxyphenyl)ethan-1-one
2'-Hydroxy-4',6'-dimethoxy-2-(4-methoxyphenyl)acetophenone
4’,6’-Dimethoxy-2’-hydroxy-2(4’-methoxyphenylacetophenone)

CAS:

39604-68-7

MF:

C17H18O5

MW:

302.32

Mol File:

39604-68-7.mol

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1-(2-Hydroxy-4,6-dimethoxyphenyl)-2-(4-methoxyphenyl)ethanone Chemical Properties

Melting point:: 85.0 to 89.0 °C
Boiling point:: 494.8±40.0 °C(Predicted)
Density: 1.199±0.06 g/cm3(Predicted)
solubility: soluble in Toluene
form: powder to crystal
pka: 7.07±0.40(Predicted)
color: White to Almost white
λmax: 286nm(MeOH)(lit.)
CAS DataBase Reference: 39604-68-7

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Safety Information

HS Code: 2914.50.5000

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1-(2-Hydroxy-4,6-dimethoxyphenyl)-2-(4-methoxyphenyl)ethanone Usage And Synthesis

Preparation

Preparation by partial methylation of 2,4,6-tri-hydroxyphenyl 4-methoxybenzyl ketone,
? with dimethyl sulfate in the presence of potassium carbonate in refluxing acetone, for 3 h (64%);
? with diazomethane in ethyl ether at 0° (80%) or in methanol;
? with methyl iodide in the presence of potassium carbonate in refluxing acetone for 3 h (42%).

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