1,1'-(2-Hydroxy-4,6-diMethoxy-1,3-phenylene)bis-1-propanone Chemical Properties

Melting point:

75–80°C

Boiling point:

449.9±45.0 °C(Predicted)

Density 

1.148±0.06 g/cm3(Predicted)

storage temp. 

Refrigerator, under inert atmosphere

solubility 

Chloroform; Dichloromethane; Ethyl Acetate; Methanol

pka

5.69±0.50(Predicted)

form 

Crystals

color 

Pale yellow

1,1'-(2-Hydroxy-4,6-diMethoxy-1,3-phenylene)bis-1-propanone Usage And Synthesis

Chemical Properties

White Solid

Uses

1,1'-(2-Hydroxy-4,6-dimethoxy-1,3-phenylene)bis-1-propanone is a reactant used in the preparation of Stigmatellin A (S686780).

Uses

1,1''-(2-Hydroxy-4,6-dimethoxy-1,3-phenylene)bis-1-propanone is a reactant used in the preparation of Stigmatellin A (S686780).

Preparation

Obtained by reaction of propionic acid with phloroglucinol dimethyl ether in the presence of polyphosphoric acid at 60° for 1 h (41%).