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NICKEL IODIDE

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NICKEL IODIDE Basic information

Product Name:
NICKEL IODIDE
Synonyms:
  • NICKEL(II) IODIDE
  • NICKEL IODIDE
  • NICKEL IODIDE (OUS)
  • nickel(2+)iodide
  • nickeldiiodide
  • nickeliodide(nii2)
  • nickeliodide(nii2)[qr]
  • nickelousiodide
CAS:
13462-90-3
MF:
I2Ni
MW:
312.5
EINECS:
236-666-6
Product Categories:
  • Crystal Grade Inorganics
  • Materials Science
  • Metal and Ceramic Science
  • Nickel
  • Nickel Salts
  • Catalysis and Inorganic Chemistry
  • Crystal Grade Inorganics
  • Metal and Ceramic Science
  • Nickel Salts
  • NickelMetal and Ceramic Science
  • Salts
  • Catalysis and Inorganic Chemistry
  • Chemical Synthesis
  • Chemical Synthesis
  • metal halide
Mol File:
13462-90-3.mol
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NICKEL IODIDE Chemical Properties

Melting point:
797 °C(lit.)
Boiling point:
sublimes [LID94]
Density 
5.83 g/mL at 25 °C(lit.)
storage temp. 
Keep in dark place,Inert atmosphere,Room temperature
solubility 
H2O: slightly soluble(lit.)
form 
Powder
color 
black
Specific Gravity
5.834
Water Solubility 
Soluble in water and alcohols.
Sensitive 
Hygroscopic
Merck 
13,6535
Exposure limits
ACGIH: TWA 0.1 mg/m3
NIOSH: IDLH 10 mg/m3; TWA 0.015 mg/m3
Stability:
hygroscopic
CAS DataBase Reference
13462-90-3(CAS DataBase Reference)
EPA Substance Registry System
Nickel iodide (NiI2) (13462-90-3)
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Safety Information

Hazard Codes 
T
Risk Statements 
45-61-42/43
Safety Statements 
53-22-26-36/37/39-45
RIDADR 
UN 3260 8/PG 2
WGK Germany 
3
TSCA 
Yes
HazardClass 
6.1(b)
PackingGroup 
III
HS Code 
2827600090
Hazardous Substances Data
13462-90-3(Hazardous Substances Data)

MSDS

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NICKEL IODIDE Usage And Synthesis

Chemical Properties

Black, crystalline powder or blue-green crystals; hygroscopic.Soluble in alcohol and water.

Uses

Strongly accelerates Sml2 mediated homocoupling of imines into vicinal diamines and heterocoupling reactions between imines and ketones.1

Uses

Nickel Diiodide is used in preparation of Nickel complexes for migratory reductive cross-coupling.

Uses

Strongly accelerates Sml2 mediated homocoupling of imines into vicinal diamines and heterocoupling reactions between imines and ketones.

Preparation

Nickel iodide can be prepared by dehydration of the hexahydrate or by the metathetic reaction between sodium iodide and nickel(II) chloride or nitrate in ethanol. It has the CdCl2 type lattice and is paramagnetic down to 75°K. Only one hydrate is well characterized—the blue-green NiI2?6H20 ; unlike the other halide hexahydrates, this contains [Ni(H2O)6]2+ cations.

Hazard

Toxic by ingestion.

NICKEL IODIDESupplier

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