Basic information Safety Supplier Related

(3-BROMO-5-CHLORO-PHENYL)-(5-CHLORO-2-METHOXY-PHENYL)-METHANONE

Basic information Safety Supplier Related

(3-BROMO-5-CHLORO-PHENYL)-(5-CHLORO-2-METHOXY-PHENYL)-METHANONE Basic information

Product Name:
(3-BROMO-5-CHLORO-PHENYL)-(5-CHLORO-2-METHOXY-PHENYL)-METHANONE
Synonyms:
  • (3-BROMO-5-CHLORO-PHENYL)-(5-CHLORO-2-METHOXY-PHENYL)-METHANONE
  • Methanone, (3-bromo-5-chlorophenyl)(5-chloro-2-methoxyphenyl)-
CAS:
329944-59-4
MF:
C14H9BrCl2O2
MW:
360.03
Mol File:
Mol File
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(3-BROMO-5-CHLORO-PHENYL)-(5-CHLORO-2-METHOXY-PHENYL)-METHANONE Chemical Properties

Boiling point:
479.3±45.0 °C(Predicted)
Density 
1.554±0.06 g/cm3(Predicted)
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(3-BROMO-5-CHLORO-PHENYL)-(5-CHLORO-2-METHOXY-PHENYL)-METHANONE Usage And Synthesis

Preparation

A solution of 1,3-dibromo-5-chlorobenzene (1 mmol) in ethyl ether was cooled to ?78° and n-butyllithium in hexane (1.1 mmol) was added over 2 min.The reaction mixture was stirred at ?78° for an additional 10 min, and then 5-chloro-N,2-dimethoxy-N-methylbenzamide (1 mmol) was added in small portions over 4 min. The reaction mixture was stirred at ?78° for 1.25 h and then allowed to warm to r.t. and stirred for 14 h (97%).

(3-BROMO-5-CHLORO-PHENYL)-(5-CHLORO-2-METHOXY-PHENYL)-METHANONESupplier

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