ChemicalBook > Product Catalog > Pharmaceutical intermediates > Heterocyclic compound > Pyrimidines > Methylpyrimidine > 4,4'-BIS(2-AMINO-6-METHYLPYRIMIDYL) DISULFIDE
4,4'-BIS(2-AMINO-6-METHYLPYRIMIDYL) DISULFIDE
4,4'-BIS(2-AMINO-6-METHYLPYRIMIDYL) DISULFIDE Basic information
- Product Name:
- 4,4'-BIS(2-AMINO-6-METHYLPYRIMIDYL) DISULFIDE
- Synonyms:
-
- 4,4'-BIS(2-AMINO-6-METHYLPYRIMIDYL) DISULFIDE
- bisaminomethylpyrimidyldisulfide
- 4-[(2-amino-6-methylpyrimidin-4-yl)disulfanyl]-6-methylpyrimidin-2-amine
- 2-Pyrimidinamine, 4,4'-dithiobis[6-methyl-
- 4,4'-BIS(2-AMINO-6-METHYLPYRIMIDYL) DISULFIDE ISO 9001：2015 REACH
- 6,6'-Disulfanediylbis(4-methylpyrimidin-2-amine)
- CAS:
- 69945-13-7
- MF:
- C10H12N6S2
- MW:
- 280.37
- Mol File:
- 69945-13-7.mol
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4,4'-BIS(2-AMINO-6-METHYLPYRIMIDYL) DISULFIDE Chemical Properties
- Melting point:
- 208 °C
- solubility
- sol benzene, acetonitrile.
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4,4'-BIS(2-AMINO-6-METHYLPYRIMIDYL) DISULFIDE Usage And Synthesis
Uses
4,4'-Bis(2-amino-6-methylpyrimidyl) disulfide can bind to phosphine and induce lactonization of o-hydroxy acids.
Preparation
4,4'-BIS(2-AMINO-6-METHYLPYRIMIDYL) DISULFIDE is readily prepared from commercially available 2-amino-4-chloro-6- methylpyrimidine, which is treated with NaS.H2O (5 equiv) in degassed propylene glycol at 140 °C for 3 h. The solution is diluted with H2O and neutralized with acetic acid. The collected precipitate is recrystallized from ethanol, giving pure 2-amino-4-mercapto-6-methylpyrimidine, which is dimerized with iodine in boiling methanol containing potassium carbonate.
4,4'-BIS(2-AMINO-6-METHYLPYRIMIDYL) DISULFIDESupplier
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