2-NAPHTHYL PHOSPHATE MONOSODIUM SALT Chemical Properties

storage temp. 

-20°C

BRN 

3779148

CAS DataBase Reference

14463-68-4(CAS DataBase Reference)

Safety Information

Hazard Codes 

Xi,C,F

Risk Statements 

36/37/38-34-11

Safety Statements 

26-36-45-36/37/39-16

WGK Germany 

3

F 

10-21

MSDS

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2-NAPHTHYL PHOSPHATE MONOSODIUM SALT Usage And Synthesis

Form

Powder

Uses

2-Naphthyl Phosphate, Monosodium Salt can be used as reagent/reactant in preparation mono, di and tri-?mannopyranosyl phosphates as mannose-?1-?phosphate prodrugs for potential CDG-?Ia therapy.

Purification Methods

Recrystallise it from H2O (10mL) containing NaCl (0.4g). The salt is collected by centrifugation and dried in a vacuum desiccator, m 203-205o (partially resolidifies and re-melts at 244o). It crystallises from MeOH (m 222-223o). The free acid is recrystallised several times by addition of 2.5 parts of hot CHCl3 to a hot solution of the free acid (1 part) in Me2CO (1.3 parts), m 177-178o. [Friedman & Seligmann J Am Chem Soc 73 5292 1951, Chanley & Feaggeson J Am Chem Soc 77 4002 1955, Beilstein 6 H 647, 6 III 2989, 6 IV 428.] See also entry on p 688 in Chapter 6.

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