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3-(Methoxymethylene)-2,4-bis(trimethylsilyloxy)-1,4-pentadiene

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3-(Methoxymethylene)-2,4-bis(trimethylsilyloxy)-1,4-pentadiene Basic information

Product Name:
3-(Methoxymethylene)-2,4-bis(trimethylsilyloxy)-1,4-pentadiene
Synonyms:
  • 3-(Methoxymethylene)-2,4-bis(trimethylsilyloxy)-1,4-pentadiene
  • 3,7-Dioxa-2,8-disilanonane, 5-(methoxymethylene)-2,2,8,8-tetramethyl-4,6-bis(methylene)-
CAS:
90330-49-7
MF:
C13H26O3Si2
MW:
286.51
Mol File:
90330-49-7.mol
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3-(Methoxymethylene)-2,4-bis(trimethylsilyloxy)-1,4-pentadiene Chemical Properties

Boiling point:
72 °C(Press: 2 Torr)
Density 
0.904±0.06 g/cm3(Predicted)
solubility 
very sol most organic solvents; decomposition occurs in protic solvents.
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3-(Methoxymethylene)-2,4-bis(trimethylsilyloxy)-1,4-pentadiene Usage And Synthesis

Uses

Used as a reagent for reiterative Diels-Alder reactions.

Synthesis

3-(Methoxymethylene)-2,4-bis(trimethylsilyloxy)-1,4-pentadiene is prepared by the bissilylation of 3-(methoxymethylene)-2,4-pentanedione using Chlorotrimethylsilane, dry Zinc Chloride, and Triethylamine.

storage

Stored safely for a few weeks in a refrigerator under nitrogen atmosphere; hydrolytic conditions should be avoided for reactions and handling.

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