Basic information Safety Supplier Related

D(-)3-PHOSPHOGLYCERIC ACID DISODIUM SALT

Basic information Safety Supplier Related

D(-)3-PHOSPHOGLYCERIC ACID DISODIUM SALT Basic information

Product Name:
D(-)3-PHOSPHOGLYCERIC ACID DISODIUM SALT
Synonyms:
  • D(-)3-PHOSPHOGLYCERIC ACID DISODIUM SALT
  • D-3-PHOSPHOGLYCERIC ACID DISODIUM SALT
  • D-3-Phosphoglyceric acid dissodium salt
  • D(-)3-PHOSPHOGLYCERIC ACID DISODIUM
  • D-Glycerate 3-phosphate disodium salt
  • (R)-2-hydroxy-3-(phosphonooxy)propanoic acid, disodium salt
  • D-()-3-Phosphoglyceric Acid (sodium salt)
  • disodium 3-(hydrogen phosphonooxy)-2-hydroxypropanoate
CAS:
80731-10-8
MF:
C3H8NaO7P
MW:
210.05
Mol File:
80731-10-8.mol
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D(-)3-PHOSPHOGLYCERIC ACID DISODIUM SALT Chemical Properties

Melting point:
>133°C (subl.)
storage temp. 
-20°C
solubility 
H2O: 0.1 g/mL, clear, colorless
form 
powder
color 
white
BRN 
3767836
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Safety Information

Hazard Codes 
Xi,Xn
Risk Statements 
36/37/38-68/20/21/22-20/21/22
Safety Statements 
26-36-45-36/37
WGK Germany 
3
3-10-21

MSDS

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D(-)3-PHOSPHOGLYCERIC ACID DISODIUM SALT Usage And Synthesis

Uses

D-(-)-3-Phosphoglyceric Acid Disodium Salt can be used as a hydrothermal treatment.

Biochem/physiol Actions

3-Phosphoglyceric acid is an intermediate in glycolysis. It also a precursor in the formation of serine.

Purification Methods

It is best purified by conversion to the Ba salt by precipitation with BaCl2, which is recrystallised three times before conversion to the sodium salt. The Ba salt (9.5g) is shaken with 200mL of a 1:1 slurry of Dowex 50 (Na+ form) for 2hours. The mixture is filtered, and the resin is washed with H2O (2 x 25mL). The combined filtrates (150mL) are adjusted to pH 7.0 and concentrated in vacuo to 30-40mL and filtered if not clear. Absolute EtOH is added to make 100mL, and then n-hexane is added whereby a white solid and/or a second phase separates. When set aside at room temperature, complete precipitation of the Na salt as a solid occurs. The salt is removed by centrifugation, washed with Me2CO, dried in air then in an oven at 55o to give a stable powder (4.5g). It did not lose weight when dried further over P2O5 at 78o/8hours. The high rotation in the presence of (NH4)6Mo7O24 is not very sensitive to the concentration of molybdate or pH as it did not alter appreciably in 1/3 volume between 2.5 to 25% (w/v) of molybdate or at pH values ranging between 4 and 7. [Cowgill Biochim Biophys Acta 16 613 1955, Embdan et al. Hoppe Seyler's Z Physiol Chem 230 20 1934, Beilstein 3 IV 1051.]

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