tert-Butyl monoperoxy phthalate(technically pure)
tert-Butyl monoperoxy phthalate(technically pure) Basic information
- Product Name:
- tert-Butyl monoperoxy phthalate(technically pure)
- Synonyms:
-
- tert-Butyl perophthalate
- tert-Butyl monoperoxy phthalate(technically pure)
- tert-butyl monoperphthalate
- TERT-BUTYL PEROXYPHTHALATE
- di-(tert-butylperoxy)phthalate, >= 52% as paste
- di-(tert-butylperoxy)phthalate, 43-52%
- tert-butyl monoperoxyphthalate, technical pure
- 2-(tert-Butylperoxycarbonyl)benzoic acid
- CAS:
- 15042-77-0
- MF:
- C12H14O5
- MW:
- 238.24
- EINECS:
- 239-116-3
- Mol File:
- 15042-77-0.mol
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tert-Butyl monoperoxy phthalate(technically pure) Chemical Properties
- Melting point:
- 57-57.5 °C
- Boiling point:
- 398.9±25.0 °C(Predicted)
- Density
- 1.216±0.06 g/cm3(Predicted)
- pka
- 3.30±0.36(Predicted)
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tert-Butyl monoperoxy phthalate(technically pure) Usage And Synthesis
Purification Methods
Crystallise the per acid-ester from Et2O or Et2O/pet ether and dry it over H2SO4. The ester was prepared from tert-butylhydroperoxide and phthalic anhydride [Davies et al. J Chem Soc 1545 1953]. Possibly EXPLOSIVE.[Beilstein 9 IV 3260.]