Basic information Safety Supplier Related
ChemicalBook >  Product Catalog >  Organic Chemistry >  Heterocyclic Compounds >  1-Octanoylbenzotriazole

1-Octanoylbenzotriazole

Basic information Safety Supplier Related

1-Octanoylbenzotriazole Basic information

Product Name:
1-Octanoylbenzotriazole
Synonyms:
  • N-octanoyl Benzotriazole
  • 1-(1H-Benzotriazol-1-Yl)-1-Octanone
  • 1-(1H-Benzo[d][1,2,3]triazol-1-yl)octan-1-one
  • 1-Octanone, 1-(1H-benzotriazol-1-yl)-
  • 1-(benzotriazol-1-yl)octan-1-one
CAS:
58068-80-7
MF:
C14H19N3O
MW:
245.32
Product Categories:
  • Orlistat
Mol File:
58068-80-7.mol
More
Less

1-Octanoylbenzotriazole Chemical Properties

Boiling point:
379.3±25.0 °C(Predicted)
Density 
1.12±0.1 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
solubility 
DMSO (Slightly), Methanol (Slightly)
form 
Oil
pka
-0.40±0.30(Predicted)
color 
Pale Yellow
More
Less

1-Octanoylbenzotriazole Usage And Synthesis

Uses

1-(1H-Benzotriazol-1-yl)-1-octanone is a useful intermediate, which is used in several types of reactions such as the prearation of N-acylpiperidines via acylation.

Synthesis

To a solution of 0.024 g TCT (0.130 mmol) in 2 cm3CH2Cl2 was added 0.033 g triethylamine (0.325 mmol) at0 C and the resulting mixture was stirred for 5 min.Carboxylic acid (0.271 mmol) was then added with continuouslystirring for 10 min. Subsequently, to this mixturewas added 0.032 g 1H-benzotriazole (0.271 mmol) and thesolution was allowed to warm up to room temperature andstirred until completion of the reaction based on TLCanalysis. The crude reaction mixture was extracted withsaturated NaHCO3, then washed with 1 M HCl and water.The combined organic layer was dried over anhydroussodium sulfate and concentrated under reduced pressure to afford 1-Octanoylbenzotriazole.

1-OctanoylbenzotriazoleSupplier

China Synchem Technology Co.,Ltd. Gold
Tel
+86-0552-4929304 +86-18055277008
Email
sales@cnsynchem.com
Shanghai Hanhong Scientific Co.,Ltd.
Tel
021-54306202 13764082696
Email
info@hanhongsci.com
Shanghai Topbiochem Technology Co., Ltd
Tel
+86-21-60341587
Email
sales@topbiochem.com
Shanghai JONLN Reagent Co., Ltd.
Tel
400-0066400 13621662912
Email
422131432@qq.com
Mashilabs (Shanghai) Co.,Ltd.
Tel
19916721580
Email
mafarm@126.com
More
Less

1-Octanoylbenzotriazole(58068-80-7)Related Product Information