4-(4'-BROMOPHENYL)PIPERIDINE HYDROCHLORIDE
4-(4'-BROMOPHENYL)PIPERIDINE HYDROCHLORIDE Basic information
- Product Name:
- 4-(4'-BROMOPHENYL)PIPERIDINE HYDROCHLORIDE
- Synonyms:
-
- 4-(4'-BROMOPHENYL)PIPERIDINE HYDROCHLORIDE
- 4-(4-BROMO-PHENYL)PIPERIDINE HCL
- 4-(4-bromophenyl)piperidine C11H15BrClN
- Piperidine,4-(4-bromophenyl)-, hydrochloride (1:1)
- 4-(5-bromophenyl)piperidine HCl
- CAS:
- 769944-79-8
- MF:
- C11H15BrClN
- MW:
- 276.6005
- EINECS:
- 672-425-5
- Mol File:
- 769944-79-8.mol
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4-(4'-BROMOPHENYL)PIPERIDINE HYDROCHLORIDE Chemical Properties
- storage temp.
- Inert atmosphere,Room Temperature
- Appearance
- White to off-white Powder
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4-(4'-BROMOPHENYL)PIPERIDINE HYDROCHLORIDE Usage And Synthesis
Synthesis
769944-78-7
769944-79-8
General procedure for the synthesis of 4-(4-bromophenyl)piperidine hydrochloride from 1-N-Boc-4-(4-bromophenyl)piperidine: To a solution of ethyl acetate (1 mL) containing 1-N-Boc-4-(4-bromophenyl)piperidine (1114 mg, 3.27 mmol) was slowly added a solution of ethyl acetate (2 mL) with 4 N hydrogen chloride at room temperature. The reaction mixture was stirred at room temperature for 5 h before the solvent was removed by distillation under reduced pressure. The resulting solid was washed with ethyl acetate and dried under vacuum to give 4-(4-bromophenyl)piperidine hydrochloride (884 mg, 98% yield) as a white solid.
References
[1] Patent: WO2004/85408, 2004, A1. Location in patent: Page 294
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