ChemicalBook > Product Catalog > Biochemical Engineering > Biochemical Reagents > Amines, Acids and Salts > 3-(BroMoMethyl)-5-Methylpyridine hydrobroMide
3-(BroMoMethyl)-5-Methylpyridine hydrobroMide
3-(BroMoMethyl)-5-Methylpyridine hydrobroMide Basic information
- Product Name:
- 3-(BroMoMethyl)-5-Methylpyridine hydrobroMide
- Synonyms:
-
- 3-(BroMoMethyl)-5-Methylpyridine hydrobroMide
- 3-(broMoMethyl)-5-Methylpyridine HBr
- 3-(Bromomethyl)-5-methylpyridine hydrobromide (1:1)
- Fumarate R Impurity 2
- Rupatadine impurity 4
- Fumarate Impurity 2
- -5-methylpyridine hydrobromide
- Rupatadine Impurity 6 HBr
- CAS:
- 1235342-53-6
- MF:
- C7H9Br2N
- MW:
- 266.96
- Product Categories:
-
- DCP
- Mol File:
- 1235342-53-6.mol
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3-(BroMoMethyl)-5-Methylpyridine hydrobroMide Chemical Properties
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- InChI
- InChI=1S/C7H8BrN.BrH/c1-6-2-7(3-8)5-9-4-6;/h2,4-5H,3H2,1H3;1H
- InChIKey
- CKEAZZPEMCPDPI-UHFFFAOYSA-N
- SMILES
- C(C1=CN=CC(C)=C1)Br.Br
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3-(BroMoMethyl)-5-Methylpyridine hydrobroMide Usage And Synthesis
Synthesis
102074-19-1
1235342-53-6
Step 2: Dissolve 5-methyl-3-pyridine methanol (10 mmol) in 10 mL of 40% aqueous hydrobromic acid and react at reflux for 5 h. The reaction was monitored by TLC or LC-MS. Upon completion of the reaction, the mixture was heated to remove the solvent (water and excess hydrobromic acid) by evaporation until the mixture became viscous. After cooling, acetone was added to the mixture to precipitate the product, the solid was collected by filtration and dried to give 3-(bromomethyl)-5-methylpyridine hydrobromide in up to 80% yield.
References
[1] Patent: WO2012/97196, 2012, A1. Location in patent: Page/Page column 34
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