DEUTERIUM BROMIDE
DEUTERIUM BROMIDE Basic information
- Product Name:
- DEUTERIUM BROMIDE
- Synonyms:
-
- (2H)Hydridebromine
- Hydrogen bromide (1D)
- Hydrogen bromide (D)
- Deuterium bromide, 46 wt% in Deuterium oxide
- Deuterium bromide,for NMR,47 wt. % solution in D2O, 99+ atom % D
- Deuterium bromide, 48% w/w in D2O, 99+% (Isotopic)
- Deuterium Bromide (46% weight in D2O) >99.0 Atom % D
- DBr solution
- CAS:
- 13536-59-9
- MF:
- BrD
- MW:
- 81.92
- EINECS:
- 236-894-6
- Product Categories:
-
- Chemical Synthesis
- Compressed and Liquefied GasesStable Isotopes
- NMR - Buffers and Reagents
- Alphabetical Listings
- Gases
- Synthetic Reagents
- DStable Isotopes
- NMR Solvents and Reagents
- Stable Isotopes
- Mol File:
- 13536-59-9.mol
DEUTERIUM BROMIDE Chemical Properties
- Melting point:
- −87 °C(lit.)
- Boiling point:
- 126 °C(lit.)
- Density
- 1.537 g/mL at 25 °C
- vapor density
- 2.71 (20 °C, vs air)
- vapor pressure
- 334.7 psi ( 21 °C)
- Flash point:
- 126°C
- solubility
- Water (Soluble)
- form
- Liquid
- color
- Colorless
- Water Solubility
- soluble H2O [CRC10]
- Sensitive
- Moisture Sensitive
- CAS DataBase Reference
- 13536-59-9(CAS DataBase Reference)
Safety Information
- Hazard Codes
- C,T
- Risk Statements
- 23/24/25-34-35
- Safety Statements
- 23-26-36/37/39-45
- RIDADR
- UN 1788 8/PG 2
- WGK Germany
- 3
- HazardClass
- 8
- PackingGroup
- II
- HS Code
- 2845901000
MSDS
- Language:English Provider:SigmaAldrich
- Language:English Provider:ACROS
- Language:English Provider:ALFA
DEUTERIUM BROMIDE Usage And Synthesis
Description
Deuterium bromide is stored either as a liquid at a low temperature or as a gas in a sealed glass flask. Pure DBr reacts with Hg only on long exposure.
Chemical Properties
clear colorless to slightly yellow solution
Uses
NMR Solvent
Preparation
The vacuum-sealed ampoules with the starting materials are broken by vigorous shaking in an evacuated 5-liter flask closed by a ground glass stopper with a stopcock. To complete the deuterolysis, the mixture is left standing in the dark for two days, with occasional shaking. The reaction should not be accelerated by heating or disproportionation (4 D3PO3 = 3 D3P04 + PD3) will occur, and the DBr will be contaminated with PD3. After sealing the flask to a high vacuum system, the impure gas is condensed in a receiver cooled with liquid nitrogen and purified by fractional distillation, using a low-temperature distillation flask.only half of the deuterium feed is converted to desired products.
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