2-(3-Aminophenyl)ethanol
- Product Name
- 2-(3-Aminophenyl)ethanol
- CAS No.
- 52273-77-5
- Chemical Name
- 2-(3-Aminophenyl)ethanol
- Synonyms
- 3-Aminophenethyl alcohol;2-(3-Aminophenyl)ethanol;Benzeneethanol, 3-aMino-;3-(2-Hydroxyethyl)aniline;2-(3-aminophenyl)ethanol b;2-(3-aminophenyl)ethan-1-ol;2-(3-aminophenyl)ethanol - [A86885]
- CBNumber
- CB01025910
- Molecular Formula
- C8H11NO
- Formula Weight
- 137.18
- MOL File
- 52273-77-5.mol
2-(3-Aminophenyl)ethanol Property
- Melting point:
- 51-53 ºC
- Boiling point:
- 293 ºC
- Density
- 1.124
- Flash point:
- 131 ºC
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- solubility
- DMSO (Slightly), Methanol (Slightly)
- form
- Solid
- pka
- 14.91±0.10(Predicted)
- color
- Dark Brown to Black
Safety
- HS Code
- 2922190090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H319Causes serious eye irritation
- Precautionary statements
-
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- A615645
- Product name
- 2-(3-Aminophenyl)ethanol
- Packaging
- 100mg
- Price
- $50
- Updated
- 2021/12/16
- Product number
- A615645
- Product name
- 2-(3-Aminophenyl)ethanol
- Packaging
- 250mg
- Price
- $70
- Updated
- 2021/12/16
- Product number
- A615645
- Product name
- 2-(3-Aminophenyl)ethanol
- Packaging
- 500mg
- Price
- $100
- Updated
- 2021/12/16
- Product number
- 7359AB
- Product name
- 2-(3-Aminophenyl)ethanol
- Packaging
- 1g
- Price
- $171
- Updated
- 2021/12/16
- Product number
- FA139561
- Product name
- 2-(3-Aminophenyl)ethanol
- Packaging
- 250mg
- Price
- $195
- Updated
- 2021/12/16
2-(3-Aminophenyl)ethanol Chemical Properties,Usage,Production
Uses
2-(3-Aminophenyl)ethanol is a useful compound for the synthesis of indolines and dihydrobenzofurans via iron and copper-catalyzed iodination and cyclization.
Synthesis
52022-77-2
52273-77-5
Step A: Synthesis of 2-(3-aminophenyl)ethanol To a pressure reactor was added 3-nitrophenylethanol (3.0 g, 18 mmol), methanol (100 mL) and 10% palladium carbon catalyst (0.1 g, 0.08 mmol). The reaction system was subjected to 45 psi hydrogen pressure and the reaction was stirred at room temperature overnight. Upon completion of the reaction, the catalyst was removed by filtration through a diatomaceous earth pad, and the filtrate was concentrated under reduced pressure to afford the target product 2-(3-aminophenyl)ethanol (2.44 g, 99% yield) in white solid form. The product was analyzed by LCMS to confirm that the molecular ion peak [M+H]+ m/z = 138.1, which is consistent with the theoretical value C8H11NO.
References
[1] Patent: JP5829520, 2015, B2. Location in patent: Paragraph 0356
[2] Patent: US2010/190804, 2010, A1. Location in patent: Page/Page column 63-64
[3] Patent: EP2623492, 2013, A1. Location in patent: Paragraph 0323-0324
[4] Patent: WO2006/117549, 2006, A1. Location in patent: Page/Page column 105
[5] Patent: WO2004/113282, 2004, A1. Location in patent: Page 37
2-(3-Aminophenyl)ethanol Preparation Products And Raw materials
Raw materials
Preparation Products
2-(3-Aminophenyl)ethanol Suppliers
- Tel
- --
- Fax
- --
- info@ramidus.se
- Country
- Sweden
- ProdList
- 155
- Advantage
- 50
View Lastest Price from 2-(3-Aminophenyl)ethanol manufacturers
- Product
- 2-(3-Aminophenyl)ethanol 52273-77-5
- Price
- US $1.00/g
- Min. Order
- 1g
- Purity
- ≥98%
- Supply Ability
- g/kg/Ton
- Release date
- 2020-03-05