ChemicalBook > CAS DataBase List > 5-CHLORO-1,6-NAPHTHYRIDINE

5-CHLORO-1,6-NAPHTHYRIDINE

Product Name
5-CHLORO-1,6-NAPHTHYRIDINE
CAS No.
23616-32-2
Chemical Name
5-CHLORO-1,6-NAPHTHYRIDINE
Synonyms
1,6-Naphthyridine,5-chloro-;5-Chloro-[1,6]naphthyridi...;5-Chloro-1,6-naphthyridine 95+%;5-Chloro-1,6-naphthyridine, CAS 23616-32-2
CBNumber
CB01096574
Molecular Formula
C8H5ClN2
Formula Weight
164.59
MOL File
23616-32-2.mol
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5-CHLORO-1,6-NAPHTHYRIDINE Property

Melting point:
106-107℃
Boiling point:
307.9±22.0 °C(Predicted)
Density 
1.349±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
pka
2.04±0.30(Predicted)
Appearance
Off-white to yellow Solid
CAS DataBase Reference
23616-32-2
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Safety

HazardClass 
IRRITANT
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
C611265
Product name
5-chloro-1,6-naphthyridine
Packaging
50mg
Price
$45
Updated
2021/12/16
SynQuest Laboratories
Product number
3H32-5-1L
Product name
5-Chloro-1,6-naphthyridine
Purity
95.0%
Packaging
1g
Price
$224
Updated
2021/12/16
Matrix Scientific
Product number
066704
Product name
5-Chloro-1,6-naphthyridine
Packaging
500mg
Price
$352
Updated
2021/12/16
Medical Isotopes, Inc.
Product number
37976
Product name
5-Chloro[1,6]naphthyridine
Purity
95+%
Packaging
1g
Price
$600
Updated
2021/12/16
SynQuest Laboratories
Product number
3H32-5-1L
Product name
5-Chloro-1,6-naphthyridine
Purity
95.0%
Packaging
5G
Price
$888
Updated
2021/12/16
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5-CHLORO-1,6-NAPHTHYRIDINE Chemical Properties,Usage,Production

Synthesis

23616-31-1

23616-32-2

General procedure for the synthesis of 5-chloro[1,6]diazanaphthalene from 1,6-naphthopyridin-5(6H)-one: the product of Example 36d (0.250 g, 1.71 mmol) was mixed with phosphorus trichloride (4 mL) and reacted under nitrogen protection at 80 °C for 18.5 hours. Upon completion of the reaction, the volatiles were removed by vacuum distillation. The residue was slurried with ice water and adjusted to pH 7-8 with concentrated ammonium hydroxide solution.5-Chloro[1,6]diazanaphthalene was collected by vacuum filtration, washed with water and dried under vacuum to give a gray solid (0.245 g, 87% yield) of sufficient purity to be used in subsequent separations.

References

[1] Patent: WO2008/133753, 2008, A2. Location in patent: Page/Page column 81

5-CHLORO-1,6-NAPHTHYRIDINE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 5-CHLORO-1,6-NAPHTHYRIDINE manufacturers

Nanjing jinheyou Trading Co., Ltd.
Product
5-CHLORO-1,6-NAPHTHYRIDINE 23616-32-2
Price
US $0.00/g
Min. Order
1g
Purity
95%min
Supply Ability
20kg/month
Release date
2019-12-30

23616-32-2, 5-CHLORO-1,6-NAPHTHYRIDINE Related Search:

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