5-CHLORO-1,6-NAPHTHYRIDINE
- Product Name
- 5-CHLORO-1,6-NAPHTHYRIDINE
- CAS No.
- 23616-32-2
- Chemical Name
- 5-CHLORO-1,6-NAPHTHYRIDINE
- Synonyms
- 1,6-Naphthyridine,5-chloro-;5-Chloro-[1,6]naphthyridi...;5-Chloro-1,6-naphthyridine 95+%;5-Chloro-1,6-naphthyridine, CAS 23616-32-2
- CBNumber
- CB01096574
- Molecular Formula
- C8H5ClN2
- Formula Weight
- 164.59
- MOL File
- 23616-32-2.mol
5-CHLORO-1,6-NAPHTHYRIDINE Property
- Melting point:
- 106-107℃
- Boiling point:
- 307.9±22.0 °C(Predicted)
- Density
- 1.349±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- pka
- 2.04±0.30(Predicted)
- Appearance
- Off-white to yellow Solid
- CAS DataBase Reference
- 23616-32-2
Safety
- HazardClass
- IRRITANT
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- C611265
- Product name
- 5-chloro-1,6-naphthyridine
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- 3H32-5-1L
- Product name
- 5-Chloro-1,6-naphthyridine
- Purity
- 95.0%
- Packaging
- 1g
- Price
- $224
- Updated
- 2021/12/16
- Product number
- 066704
- Product name
- 5-Chloro-1,6-naphthyridine
- Packaging
- 500mg
- Price
- $352
- Updated
- 2021/12/16
- Product number
- 37976
- Product name
- 5-Chloro[1,6]naphthyridine
- Purity
- 95+%
- Packaging
- 1g
- Price
- $600
- Updated
- 2021/12/16
- Product number
- 3H32-5-1L
- Product name
- 5-Chloro-1,6-naphthyridine
- Purity
- 95.0%
- Packaging
- 5G
- Price
- $888
- Updated
- 2021/12/16
5-CHLORO-1,6-NAPHTHYRIDINE Chemical Properties,Usage,Production
Synthesis
23616-31-1
23616-32-2
General procedure for the synthesis of 5-chloro[1,6]diazanaphthalene from 1,6-naphthopyridin-5(6H)-one: the product of Example 36d (0.250 g, 1.71 mmol) was mixed with phosphorus trichloride (4 mL) and reacted under nitrogen protection at 80 °C for 18.5 hours. Upon completion of the reaction, the volatiles were removed by vacuum distillation. The residue was slurried with ice water and adjusted to pH 7-8 with concentrated ammonium hydroxide solution.5-Chloro[1,6]diazanaphthalene was collected by vacuum filtration, washed with water and dried under vacuum to give a gray solid (0.245 g, 87% yield) of sufficient purity to be used in subsequent separations.
References
[1] Patent: WO2008/133753, 2008, A2. Location in patent: Page/Page column 81
5-CHLORO-1,6-NAPHTHYRIDINE Preparation Products And Raw materials
Raw materials
Preparation Products
5-CHLORO-1,6-NAPHTHYRIDINE Suppliers
- Tel
- --
- Fax
- --
- sales@ajchem.in
- Country
- India
- ProdList
- 6100
- Advantage
- 58
View Lastest Price from 5-CHLORO-1,6-NAPHTHYRIDINE manufacturers
- Product
- 5-CHLORO-1,6-NAPHTHYRIDINE 23616-32-2
- Price
- US $0.00/g
- Min. Order
- 1g
- Purity
- 95%min
- Supply Ability
- 20kg/month
- Release date
- 2019-12-30