3-NITRO-6,7-DIHYDRO-5H-CYCLOPENTA[B]PYRIDINE
- Product Name
- 3-NITRO-6,7-DIHYDRO-5H-CYCLOPENTA[B]PYRIDINE
- CAS No.
- 84531-36-2
- Chemical Name
- 3-NITRO-6,7-DIHYDRO-5H-CYCLOPENTA[B]PYRIDINE
- Synonyms
- 3-nitro-5H,6H,7H-cyclopenta[b]pyridine;3-NITRO-6,7-DIHYDRO-5H-CYCLOPENTA[B]PYRIDINE;6,7-dihydro-3-nitro-5H-Cyclopenta[b]pyridine;5H-Cyclopenta[b]pyridine,6,7-dihydro-3-nitro-;3-NITRO-6,7-DIHYDRO-5H-CYCLOPENTA[B]PYRIDINE ISO 9001:2015 REACH
- CBNumber
- CB01253478
- Molecular Formula
- C8H8N2O2
- Formula Weight
- 164.16
- MOL File
- 84531-36-2.mol
3-NITRO-6,7-DIHYDRO-5H-CYCLOPENTA[B]PYRIDINE Property
- Melting point:
- 94-95 °C
- Boiling point:
- 277.9±40.0 °C(Predicted)
- Density
- 1.328±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 2.15±0.20(Predicted)
- Appearance
- Light yellow to yellow Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- N901215
- Product name
- 3-Nitro-6,7-dihydro-5H-cyclopenta[b]pyridine
- Packaging
- 100mg
- Price
- $330
- Updated
- 2021/12/16
- Product number
- W8722
- Product name
- 3-Nitro-6,7-dihydro-5H-cyclopenta[b]pyridine
- Packaging
- 1g
- Price
- $177
- Updated
- 2021/12/16
- Product number
- CHM0382606
- Product name
- 3-NITRO-6,7-DIHYDRO-5H-CYCLOPENTA[B]PYRIDINE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $500.01
- Updated
- 2021/12/16
- Product number
- W8722
- Product name
- 3-Nitro-6,7-dihydro-5H-cyclopenta[b]pyridine
- Packaging
- 5g
- Price
- $555
- Updated
- 2021/12/16
- Product number
- 085984
- Product name
- 3-Nitro-6,7-dihydro-5H-cyclopenta[b]pyridine
- Purity
- 97%
- Packaging
- 1g
- Price
- $1517
- Updated
- 2021/12/16
3-NITRO-6,7-DIHYDRO-5H-CYCLOPENTA[B]PYRIDINE Chemical Properties,Usage,Production
Synthesis
14150-94-8
120-92-3
84531-36-2
GENERAL METHOD: 1-methyl-3,5-dinitro-1H-pyridin-2-one (50 mg, 0.25 mmol) was dissolved in ethanol (5 mL), followed by cyclopentanone (26 μL, 0.25 mmol) and ammonium acetate (289 mg, 3.75 mmol). The reaction mixture was heated in an oil bath at 65 °C for 24 hours. After completion of the reaction, the solvent was removed by rotary evaporation and the residue was washed with benzene (3 × 10 mL) to afford 3-nitro-6,7-dihydro-5-hydro-cyclopenta[b]pyridine (42 mg, 0.24 mmol, 95% yield) as a yellow powder. The reaction of other ketones with 1-methyl-3,5-dinitro-1H-pyridin-2-one was carried out according to similar conditions. When microwave heating was used, the reaction conditions were the same as described above.
References
[1] Synthesis (Germany), 2014, vol. 46, # 16, p. 2175 - 2178
[2] Bulletin of the Chemical Society of Japan, 1990, vol. 63, # 10, p. 2820 - 2827
3-NITRO-6,7-DIHYDRO-5H-CYCLOPENTA[B]PYRIDINE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 3-NITRO-6,7-DIHYDRO-5H-CYCLOPENTA[B]PYRIDINE manufacturers
- Product
- 3-NITRO-6,7-DIHYDRO-5H-CYCLOPENTA[B]PYRIDINE 84531-36-2
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.0% min
- Supply Ability
- 100 tons min
- Release date
- 2021-05-13