1H-Imidazole-2-carboxylicacid,1-methyl-,methylester(9CI)
- Product Name
- 1H-Imidazole-2-carboxylicacid,1-methyl-,methylester(9CI)
- CAS No.
- 62366-53-4
- Chemical Name
- 1H-Imidazole-2-carboxylicacid,1-methyl-,methylester(9CI)
- Synonyms
- methyl 1-methylimidazole-2-carboxylate;1,2-Propanediol,3-(3,10-dimethylphenoxy)-;Methyl 1-Methyl-1H-iMidazole-2-carboxylate;1-methyl-1H-Imidazole-2-carboxylic acid methyl ester;1H-Imidazole-2-carboxylic acid, 1-methyl-, methyl ester;1H-Imidazole-2-carboxylicacid,1-methyl-,methylester(9CI)
- CBNumber
- CB01278626
- Molecular Formula
- C6H8N2O2
- Formula Weight
- 140.14
- MOL File
- 62366-53-4.mol
1H-Imidazole-2-carboxylicacid,1-methyl-,methylester(9CI) Property
- Boiling point:
- 90-94℃/0.6Torr
- Density
- 1.18±0.1 g/cm3(Predicted)
- storage temp.
- 2-8°C
- pka
- 4.00±0.25(Predicted)
- Appearance
- Light yellow to yellow Liquid
Safety
- HS Code
- 2933299090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- OR910010
- Product name
- Methyl1-methyl-1H-imidazole-2-carboxylate
- Purity
- 95%
- Packaging
- 1g
- Price
- $85
- Updated
- 2021/12/16
- Product number
- 123809
- Product name
- Methyl1-methyl-1H-imidazole-2-carboxylate
- Purity
- 95+%
- Packaging
- 1g
- Price
- $100
- Updated
- 2021/12/16
- Product number
- OR910010
- Product name
- Methyl1-methyl-1H-imidazole-2-carboxylate
- Purity
- 95%
- Packaging
- 10g
- Price
- $245
- Updated
- 2021/12/16
- Product number
- OR910010
- Product name
- Methyl1-methyl-1H-imidazole-2-carboxylate
- Purity
- 95%
- Packaging
- 25g
- Price
- $490
- Updated
- 2021/12/16
- Product number
- CHM0313641
- Product name
- METHYL-1-METHYL-1H-IMIDAZOLE-2-CARBOXYLATE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $500.05
- Updated
- 2021/12/16
1H-Imidazole-2-carboxylicacid,1-methyl-,methylester(9CI) Chemical Properties,Usage,Production
Synthesis
616-47-7
79-22-1
62366-53-4
In a 100 mL three-necked flask protected with argon, 22 mL of acetonitrile and 6.3 mL of methyl chloroformate were added and the mixture was cooled to -20°C. A solution of 3.3 g N-methylimidazole and 6.8 mL triethylamine dissolved in 8 mL of acetonitrile was slowly added dropwise for a controlled time of 30 minutes. After the dropwise addition, the reaction mixture was stirred at room temperature for 12 hours. After completion of the reaction, 50 mL of ethyl acetate was added to the reaction solution, the insoluble material was removed by filtration and the solid residue was washed with 50 mL of ethyl acetate. The filtrate and washings were combined and concentrated under reduced pressure. The resulting crude product was purified by silica gel column chromatography with the eluent being a mixed solvent of hexane/ethyl acetate to give 4.2 g of methyl 1-methyl-1H-imidazole-2-carboxylate in 73% yield.
References
[1] Patent: JP2017/66077, 2017, A. Location in patent: Paragraph 0059
1H-Imidazole-2-carboxylicacid,1-methyl-,methylester(9CI) Preparation Products And Raw materials
Raw materials
Preparation Products
1H-Imidazole-2-carboxylicacid,1-methyl-,methylester(9CI) Suppliers
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View Lastest Price from 1H-Imidazole-2-carboxylicacid,1-methyl-,methylester(9CI) manufacturers
- Product
- 1H-Imidazole-2-carboxylicacid,1-methyl-,methylester(9CI) 62366-53-4
- Price
- US $2.00/KG
- Min. Order
- 1g
- Purity
- 98%min
- Supply Ability
- ask
- Release date
- 2020-01-08