1H-Indole-3-carboxamide(9CI)

Product Name: 1H-Indole-3-carboxamide(9CI)
CAS No.: 1670-85-5
Chemical Name: 1H-Indole-3-carboxamide(9CI)
Synonyms: 1H-Indole-3-carboxamide(9CI);indole-3-yl carboxylic acid amide;2,6-Piperidinedione,3-[(6-chlorophenyl)methyl]-
CBNumber: CB01282935
Molecular Formula: C9H8N2O
Formula Weight: 160.17
MOL File: 1670-85-5.mol

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1H-Indole-3-carboxamide(9CI) Property

Melting point:: 201 °C
Boiling point:: 457.6±18.0 °C(Predicted)
Density: 1.328±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 15.80±0.30(Predicted)
Appearance: Off-white to light brown Solid

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Safety

HS Code: 2933998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P330Rinse mouth.

P403+P233Store in a well-ventilated place. Keep container tightly closed.

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: I629028
Product name: 1H-Indole-3-carboxylicAcidAmide
Packaging: 100mg
Price: $65
Updated: 2021/12/16

AK Scientific

Product number: W3631
Product name: 1H-Indole-3-carboxylicacidamide
Packaging: 1g
Price: $192
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0077922
Product name: 1H-INDOLE-3-CARBOXYLIC ACID AMIDE
Purity: 95.00%
Packaging: 1G
Price: $808.89
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0077922
Product name: 1H-INDOLE-3-CARBOXYLIC ACID AMIDE
Purity: 95.00%
Packaging: 2.5G
Price: $1147.43
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0077922
Product name: 1H-INDOLE-3-CARBOXYLIC ACID AMIDE
Purity: 95.00%
Packaging: 5G
Price: $1421.65
Updated: 2021/12/16

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1H-Indole-3-carboxamide(9CI) Chemical Properties,Usage,Production

Synthesis

5457-28-3

1670-85-5

GENERAL METHOD: To an anhydrous ethanol solution of 3-cyanoindole (15 mmol) was added 40% aqueous NaOH (5 mL) under stirring conditions. The reaction process was monitored by thin layer chromatography (TLC). Subsequently, 30% aqueous H2O2 solution (10.5 mL, 104.7 mmol) was slowly added dropwise to the reaction mixture. Upon completion of the reaction, the precipitated solid was collected by filtration, washed with water and recrystallized with anhydrous ethanol. Finally, the product was dried under vacuum to give 1H-indole-3-carboxamide (20a). The product was a white solid in 75% yield with a melting point of 195-197 °C (literature value 197-199 °C [31]).1H NMR (δ, ppm): 6.84 (s, 1H, NH), 7.13-7.21 (m, 2H, ArH), 7.47 (d, J = 8.0 Hz, 2H, ArH), 8.08 (s, 1H, NH), 8.20 (d, J = 7.5 Hz, 1H, ArH), 11.60 (s, 1H, NH).

References

[1] Applied Organometallic Chemistry, 2014, vol. 28, # 12, p. 900 - 907
[2] Catalysis Science and Technology, 2015, vol. 5, # 3, p. 1606 - 1622
[3] Synthetic Communications, 2013, vol. 43, # 21, p. 2867 - 2875
[4] Dalton Transactions, 2016, vol. 45, # 34, p. 13590 - 13603
[5] Russian Journal of General Chemistry, 2017, vol. 87, # 12, p. 3006 - 3016

1H-Indole-3-carboxamide(9CI) Preparation Products And Raw materials

Raw materials

Preparation Products

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1H-Indole-3-carboxamide(9CI) Suppliers

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1670-85-5, 1H-Indole-3-carboxamide(9CI)Related Search:

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1H-Indole-3-carboxamide(9CI)

indole-3-yl carboxylic acid amide

2,6-Piperidinedione,3-[(6-chlorophenyl)methyl]-

1670-85-5

AMIDE