2-ALLYLOXYBENZALDEHYDE
- Product Name
- 2-ALLYLOXYBENZALDEHYDE
- CAS No.
- 28752-82-1
- Chemical Name
- 2-ALLYLOXYBENZALDEHYDE
- Synonyms
- VHR BO2U1;NSC 406724;AKOS B005827;ASISCHEM V41613;TIMTEC-BB SBB007636;2-ALLYLOXYBENZALDEHYDE;O-ALLYLOXYBENZALDEHYDE;2-Allylpxybenzaldehyde;O-Allylsalicylaldehyde;2-Allyloxybenzaldehyde,90%
- CBNumber
- CB0133559
- Molecular Formula
- C10H10O2
- Formula Weight
- 162.19
- MOL File
- 28752-82-1.mol
2-ALLYLOXYBENZALDEHYDE Property
- Boiling point:
- 130 °C/10 mmHg (lit.)
- Density
- 1.079 g/mL at 25 °C (lit.)
- refractive index
- 1.554-1.556
- Flash point:
- 109 °C
- storage temp.
- Inert atmosphere,2-8°C
- form
- clear liquid
- color
- Colorless to Light yellow to Light orange
- Specific Gravity
- 1.079
- Sensitive
- Air Sensitive
- InChIKey
- BXCJDECTRRMSCV-UHFFFAOYSA-N
- CAS DataBase Reference
- 28752-82-1(CAS DataBase Reference)
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
N-Bromosuccinimide Price
- Product number
- 445509
- Product name
- 2-Allyloxybenzaldehyde
- Purity
- technical grade
- Packaging
- 5ml
- Price
- $105
- Updated
- 2023/06/20
- Product number
- 445509
- Product name
- 2-Allyloxybenzaldehyde
- Purity
- technical grade
- Packaging
- 25ml
- Price
- $385
- Updated
- 2023/06/20
- Product number
- A1515
- Product name
- 2-Allyloxybenzaldehyde
- Purity
- >96.0%(GC)
- Packaging
- 5g
- Price
- $80
- Updated
- 2025/07/31
- Product number
- A1515
- Product name
- 2-Allyloxybenzaldehyde
- Purity
- >96.0%(GC)
- Packaging
- 25g
- Price
- $317
- Updated
- 2025/07/31
- Product number
- A561785
- Product name
- 2-Allyloxybenzaldehyde
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
2-ALLYLOXYBENZALDEHYDE Chemical Properties,Usage,Production
Chemical Properties
clear yellow to orange liquid
Synthesis
90-02-8
106-95-6
28752-82-1
Salicylaldehyde (0.5 mL, 4.69 mmol, Sigma-Aldrich Catalog No. S356) was dissolved in acetonitrile (10 mL), followed by the addition of potassium carbonate (0.97 mL, 7.03 mmol) and 3-bromo-1-propene (0.45 mL, 5.16 mmol, Sigma-Aldrich Catalog No. 337528). The reaction mixture was stirred under reflux conditions for 12 hours. Upon completion of the reaction, the solvent was removed by vacuum evaporation and the residue was dissolved in ethyl acetate (5 mL). Water (10 mL) was added and stirred for 10 min at room temperature. The organic phase was separated and the aqueous layer was extracted with ethyl acetate (2 x 10 mL). The organic phases were combined, dried with anhydrous sodium sulfate, filtered and concentrated under reduced pressure to give o-propenyloxybenzaldehyde in 99% yield. The product was extracted by 1H NMR (400 MHz, CDCl3) δ= 10.25 (1H, s), 7.54-7.52 (1H, m), 7.23-7.19 (1H, m), 6.72-6.66 (2H, m), 5.82-5.75 (1H, m), 5.20-5.15 (1H, d, J = 17.6 Hz), 5.05 -5.03 (1H, d, J = 10.8 Hz), 4.33-4.31 (2H, m) ppm; 13C NMR (CDCl3) δ 188.9,160.6,135.6,132.2,127.8,124.7,120.5,117.5,112.7,68.7 ppm; Liquid Chromatography Mass Spectrometry (LCMS) m/z z (ES+) m/z: 347.0 [2M + Na]+, 185.0 [M + Na]+, 163.0 [M + H]+; Elemental Analysis: C10H10O2: Calculated value C 74.06, H 6.21; Measured value C 74.36, H 6.52.
References
[1] European Journal of Medicinal Chemistry, 2010, vol. 45, # 11, p. 5265 - 5277
[2] Angewandte Chemie - International Edition, 2009, vol. 48, # 51, p. 9690 - 9692
[3] Angewandte Chemie - International Edition, 2011, vol. 50, # 26, p. 5932 - 5937
[4] Chemistry - A European Journal, 2013, vol. 19, # 47, p. 15852 - 15855
[5] Tetrahedron Letters, 1995, vol. 36, # 11, p. 1845 - 1848
2-ALLYLOXYBENZALDEHYDE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 2-ALLYLOXYBENZALDEHYDE manufacturers
- Product
- 2-ALLYLOXYBENZALDEHYDE 28752-82-1
- Price
- US $0.00-0.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20 mt
- Release date
- 2025-03-14
- Product
- 2-Allyloxybenzaldehyde 28752-82-1
- Price
- US $0.00-0.00/g
- Min. Order
- 10mg
- Purity
- 99%HPLC
- Supply Ability
- 2000tons
- Release date
- 2020-01-15
- Product
- 2-ALLYLOXYBENZALDEHYDE 28752-82-1
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-08-10