6-bromocinnoline
- Product Name
- 6-bromocinnoline
- CAS No.
- 318276-72-1
- Chemical Name
- 6-bromocinnoline
- Synonyms
- 6-bromocinnoline;Cinnoline, 6-bromo-
- CBNumber
- CB01458264
- Molecular Formula
- C8H5BrN2
- Formula Weight
- 209.04
- MOL File
- 318276-72-1.mol
6-bromocinnoline Property
- Melting point:
- 129-130 °C
- Boiling point:
- 325.0±34.0 °C(Predicted)
- Density
- 1.656±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 1.75±0.10(Predicted)
- Appearance
- black powder
- CAS DataBase Reference
- 318276-72-1
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
P403+P233Store in a well-ventilated place. Keep container tightly closed.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- B614190
- Product name
- 6-Bromocinnoline
- Packaging
- 10mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- 3488AB
- Product name
- 6-Bromocinnoline
- Packaging
- 250mg
- Price
- $228
- Updated
- 2021/12/16
- Product number
- HCH0359744
- Product name
- 6-BROMOCINNOLINE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $502.43
- Updated
- 2021/12/16
- Product number
- 3488AB
- Product name
- 6-Bromocinnoline
- Packaging
- 5g
- Price
- $1883
- Updated
- 2021/12/16
- Product number
- A143870
- Product name
- 6-Bromocinnoline
- Purity
- 95%
- Packaging
- 100mg
- Price
- $82
- Updated
- 2021/12/16
6-bromocinnoline Chemical Properties,Usage,Production
Synthesis
552330-88-8
318276-72-1
Synthesis of Example 34F 6-Bromocinnoline: Example 34E (3.5 g, 14 mmol) was dissolved in water (50 mL) and heated to reflux. Subsequently, a solution of CuSO4 (2.8 g, 17.5 mmol) in water (20 mL) was added slowly dropwise to the reaction system and kept at reflux for 2 hours. After completion of the reaction, the reaction was cooled to room temperature and the pH was adjusted with saturated aqueous NaHCO3 solution to 7. The reaction mixture was extracted with ethyl acetate (2 x 25 mL), the organic phases were combined and concentrated. The crude product was purified by fast column chromatography on silica gel with the eluent being a 1:1 hexane/ethyl acetate solvent mixture to give the final target product 6-bromocinnoline (0.7 g, 24% yield).
References
[1] Bioorganic and Medicinal Chemistry, 2006, vol. 14, # 20, p. 6832 - 6846
[2] Patent: US2003/187026, 2003, A1
[3] Patent: US2003/199511, 2003, A1. Location in patent: Page/Page column 27
[4] Journal of the Chemical Society, 1950, p. 392,395
6-bromocinnoline Preparation Products And Raw materials
Raw materials
Preparation Products
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