ChemicalBook > CAS DataBase List > 3-chloro-5-nitro-benzoic acid

3-chloro-5-nitro-benzoic acid

Product Name
3-chloro-5-nitro-benzoic acid
CAS No.
34662-36-7
Chemical Name
3-chloro-5-nitro-benzoic acid
Synonyms
3-Nitro-5-chlorobenzoic acid;3-chloro-5-nitro-benzoic acid;Benzoic acid, 3-chloro-5-nitro-;3-Chloro-5-nitrobenzoic acid 98%;3-Chloro-5-nitrobenzoic acid: 3-Nitro-5-chlorobenzoic acid
CBNumber
CB01458769
Molecular Formula
C7H4ClNO4
Formula Weight
201.56
MOL File
34662-36-7.mol
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3-chloro-5-nitro-benzoic acid Property

Boiling point:
351.1±27.0 °C(Predicted)
Density 
1.602±0.06 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
pka
3.11±0.10(Predicted)
Appearance
Light yellow to brown Solid
InChI
InChI=1S/C7H4ClNO4/c8-5-1-4(7(10)11)2-6(3-5)9(12)13/h1-3H,(H,10,11)
InChIKey
YLQAJBKACBLUCM-UHFFFAOYSA-N
SMILES
C(O)(=O)C1=CC([N+]([O-])=O)=CC(Cl)=C1
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Safety

HS Code 
2916399090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
C381123
Product name
3-Chloro-5-nitrobenzoicacid
Packaging
500mg
Price
$75
Updated
2021/12/16
Apolloscientific
Product number
OR401023
Product name
3-Chloro-5-nitrobenzoicacid
Purity
98%
Packaging
5g
Price
$138
Updated
2021/12/16
Apolloscientific
Product number
OR401023
Product name
3-Chloro-5-nitrobenzoicacid
Purity
98%
Packaging
1g
Price
$37
Updated
2021/12/16
SynQuest Laboratories
Product number
4654-5-1Q
Product name
3-Chloro-5-nitrobenzoic acid
Purity
98%
Packaging
1g
Price
$40
Updated
2021/12/16
SynQuest Laboratories
Product number
4654-5-1Q
Product name
3-Chloro-5-nitrobenzoic acid
Purity
98%
Packaging
5G
Price
$152
Updated
2021/12/16
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3-chloro-5-nitro-benzoic acid Chemical Properties,Usage,Production

Uses

3-Chloro-5-nitrobenzoic acid

Synthesis

535-80-8

34662-36-7

Concentrated sulfuric acid (12 mL) was slowly added to concentrated nitric acid (1.6 mL) under cooling conditions in an ice bath and the reaction mixture was kept stirring for 5 min at 0 °C. Subsequently, 3-chlorobenzoic acid (3 g) was added in batches over 5 min, and the temperature of the reaction system was gradually brought to room temperature with continuous stirring for 1 h. The reaction was carried out in an ice bath under cooling conditions. Upon completion of the reaction, the reaction solution was slowly added dropwise to ice-cooled water, and the precipitated solid product was collected by filtration and washed thoroughly with cold water to finally obtain a white solid 3-chloro-5-nitrobenzoic acid (Compound 0004-1, 2.65 g).

References

[1] Bioorganic and Medicinal Chemistry Letters, 2013, vol. 23, # 16, p. 4557 - 4561
[2] Patent: JP6052673, 2016, B2. Location in patent: Paragraph 0081

3-chloro-5-nitro-benzoic acid Preparation Products And Raw materials

Raw materials

Preparation Products

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