2-BROMO-4-PYRIDINE ACETIC ACID

Product Name: 2-BROMO-4-PYRIDINE ACETIC ACID
CAS No.: 183483-29-6
Chemical Name: 2-BROMO-4-PYRIDINE ACETIC ACID
Synonyms: 2-Bromopyridine-4-acetic acid;2-BROMO-4-PYRIDINE ACETIC ACID;4-Pyridineacetic acid, 2-bromo-;2-(2-bromo-4-pyridyl)acetic acid
CBNumber: CB0147404
Molecular Formula: C7H6BrNO2
Formula Weight: 216.03
MOL File: 183483-29-6.mol

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2-BROMO-4-PYRIDINE ACETIC ACID Property

Melting point:: 145-150°C
Boiling point:: 374.1±27.0 °C(Predicted)
Density: 1.710±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
form: solid
pka: 3.66±0.10(Predicted)
Appearance: Off-white to brown Solid
InChI: InChI=1S/C7H6BrNO2/c8-6-3-5(1-2-9-6)4-7(10)11/h1-3H,4H2,(H,10,11)
InChIKey: SJFRXYCVLZOAEU-UHFFFAOYSA-N
SMILES: C1(Br)=NC=CC(CC(O)=O)=C1

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Safety

Hazard Codes: Xn
Risk Statements: 22
WGK Germany: 3
HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: 775967
Product name: 2-Bromopyridine-4-acetic acid
Purity: 97%
Packaging: 1g
Price: $120
Updated: 2023/06/20

American Custom Chemicals Corporation

Product number: HCH0011261
Product name: 2-BROMO-4-PYRIDINE ACETIC ACID
Purity: 95.00%
Packaging: 5G
Price: $3153.15
Updated: 2021/12/16

Ambeed

Product number: A318178
Product name: 2-(2-Bromopyridin-4-yl)aceticacid
Purity: 95+%
Packaging: 250mg
Price: $42
Updated: 2021/12/16

Ambeed

Product number: A318178
Product name: 2-(2-Bromopyridin-4-yl)aceticacid
Purity: 95+%
Packaging: 1g
Price: $95
Updated: 2021/12/16

Chemenu

Product number: CM243823
Product name: 2-(2-Bromopyridin-4-yl)aceticacid
Purity: 95%
Packaging: 1g
Price: $196
Updated: 2021/12/16

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2-BROMO-4-PYRIDINE ACETIC ACID Chemical Properties,Usage,Production

Synthesis

1256337-24-2

183483-29-6

General procedure for the synthesis of 2-(2-bromopyridin-4-yl)acetic acid from ethyl 2-(2-bromopyridin-4-yl)acetate: to a mixture of THF (5 mL), MeOH (10 mL) and water (5 mL) containing ethyl 2-(2-bromopyridin-4-yl)acetate (1.00 g, 4.10 mmol) was added lithium hydroxide (294 mg, 12.3 mmol). The reaction mixture was stirred at 20 °C for 10 min. Upon completion of the reaction, THF and MeOH were removed by vacuum concentration and the residue was diluted with 10 mL of water. Subsequently, the aqueous phase was acidified with 2N HCl solution to pH = 2. The mixture was filtered, the filter cake was collected and dried under vacuum to afford the target product 2-(2-bromopyridin-4-yl)acetic acid (850 mg, 90% yield) as a white solid.LCMS analysis resulted in (ES+) m/z (M+H)+ = 217.9 and retention time tR = 0.539 min.

References

[1] Patent: WO2018/106636, 2018, A1. Location in patent: Paragraph 00242

2-BROMO-4-PYRIDINE ACETIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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2-BROMO-4-PYRIDINE ACETIC ACID Suppliers

China 42 India 1 United Kingdom 1 United States 8 Global 52

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183483-29-6, 2-BROMO-4-PYRIDINE ACETIC ACIDRelated Search:

2-BROMO-4-PYRIDINE ACETIC ACID ethyl 2-(3-bromopyridin-4-yl)acetate 2-Bromo-4-ethylpyridine 2,2'-Bipyridine-5,5'-dicarboxylic acid

2-Bromopyridine-4-acetic acid

2-BROMO-4-PYRIDINE ACETIC ACID

4-Pyridineacetic acid, 2-bromo-

2-(2-bromo-4-pyridyl)acetic acid

183483-29-6