ChemicalBook > CAS DataBase List > 2-BROMO-4-PYRIDINE ACETIC ACID
2-BROMO-4-PYRIDINE ACETIC ACID
- Product Name
- 2-BROMO-4-PYRIDINE ACETIC ACID
- CAS No.
- 183483-29-6
- Chemical Name
- 2-BROMO-4-PYRIDINE ACETIC ACID
- Synonyms
- 2-Bromopyridine-4-acetic acid;2-BROMO-4-PYRIDINE ACETIC ACID;4-Pyridineacetic acid, 2-bromo-;2-(2-bromo-4-pyridyl)acetic acid
- CBNumber
- CB0147404
- Molecular Formula
- C7H6BrNO2
- Formula Weight
- 216.03
- MOL File
- 183483-29-6.mol
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2-BROMO-4-PYRIDINE ACETIC ACID Property
- Melting point:
- 145-150°C
- Boiling point:
- 374.1±27.0 °C(Predicted)
- Density
- 1.710±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- form
- solid
- pka
- 3.66±0.10(Predicted)
- Appearance
- Off-white to brown Solid
- InChI
- InChI=1S/C7H6BrNO2/c8-6-3-5(1-2-9-6)4-7(10)11/h1-3H,4H2,(H,10,11)
- InChIKey
- SJFRXYCVLZOAEU-UHFFFAOYSA-N
- SMILES
- C1(Br)=NC=CC(CC(O)=O)=C1
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Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
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N-Bromosuccinimide Price
Sigma-Aldrich
- Product number
- 775967
- Product name
- 2-Bromopyridine-4-acetic acid
- Purity
- 97%
- Packaging
- 1g
- Price
- $120
- Updated
- 2023/06/20
American Custom Chemicals Corporation
- Product number
- HCH0011261
- Product name
- 2-BROMO-4-PYRIDINE ACETIC ACID
- Purity
- 95.00%
- Packaging
- 5G
- Price
- $3153.15
- Updated
- 2021/12/16
Ambeed
- Product number
- A318178
- Product name
- 2-(2-Bromopyridin-4-yl)aceticacid
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $42
- Updated
- 2021/12/16
Ambeed
- Product number
- A318178
- Product name
- 2-(2-Bromopyridin-4-yl)aceticacid
- Purity
- 95+%
- Packaging
- 1g
- Price
- $95
- Updated
- 2021/12/16
Chemenu
- Product number
- CM243823
- Product name
- 2-(2-Bromopyridin-4-yl)aceticacid
- Purity
- 95%
- Packaging
- 1g
- Price
- $196
- Updated
- 2021/12/16
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2-BROMO-4-PYRIDINE ACETIC ACID Chemical Properties,Usage,Production
Synthesis
1256337-24-2
183483-29-6
General procedure for the synthesis of 2-(2-bromopyridin-4-yl)acetic acid from ethyl 2-(2-bromopyridin-4-yl)acetate: to a mixture of THF (5 mL), MeOH (10 mL) and water (5 mL) containing ethyl 2-(2-bromopyridin-4-yl)acetate (1.00 g, 4.10 mmol) was added lithium hydroxide (294 mg, 12.3 mmol). The reaction mixture was stirred at 20 °C for 10 min. Upon completion of the reaction, THF and MeOH were removed by vacuum concentration and the residue was diluted with 10 mL of water. Subsequently, the aqueous phase was acidified with 2N HCl solution to pH = 2. The mixture was filtered, the filter cake was collected and dried under vacuum to afford the target product 2-(2-bromopyridin-4-yl)acetic acid (850 mg, 90% yield) as a white solid.LCMS analysis resulted in (ES+) m/z (M+H)+ = 217.9 and retention time tR = 0.539 min.
References
[1] Patent: WO2018/106636, 2018, A1. Location in patent: Paragraph 00242
2-BROMO-4-PYRIDINE ACETIC ACID Preparation Products And Raw materials
Raw materials
Preparation Products
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183483-29-6, 2-BROMO-4-PYRIDINE ACETIC ACIDRelated Search:
2-BROMO-4-PYRIDINE ACETIC ACID
ethyl 2-(3-bromopyridin-4-yl)acetate
2-Bromo-4-ethylpyridine
2,2'-Bipyridine-5,5'-dicarboxylic acid